N⁴--N¹,N⁸-bis<2,3-(methylenedioxy)benzoyl>spermidine

Base Information

Chemical Name:N⁴--N¹,N⁸-bis<2,3-(methylenedioxy)benzoyl>spermidine
CAS No.:76927-63-4
Molecular Formula:C₃₂H₃₄N₄O₉
Molecular Weight:618.643
Hs Code.:

N<sup>4</sup>-<N-(2-Hydroxybenzoyl)glycyl>-N<sup>1</sup>,N<sup>8</sup>-bis<2,3-(methylenedioxy)benzoyl>spermidine

Synonyms:

Suppliers and Price of N⁴--N¹,N⁸-bis<2,3-(methylenedioxy)benzoyl>spermidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N⁴--N¹,N⁸-bis<2,3-(methylenedioxy)benzoyl>spermidine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N⁴--N¹,N⁸-bis<2,3-(methylenedioxy)benzoyl>spermidine

There total 4 articles about N⁴--N¹,N⁸-bis<2,3-(methylenedioxy)benzoyl>spermidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66411-55-0
2,3-(Methylenedioxy)benzoyl chloride

: 76927-63-4
N⁴--N¹,N⁸-bis<2,3-(methylenedioxy)benzoyl>spermidine

Guidance literature:: Multi-step reaction with 3 steps

1: 1,8-Bis(dimethylamino)naphthalene / CH₂Cl₂ / 16 h / Ambient temperature

2: PdCl₂ / acetic acid / Ambient temperature

3: 1,8-Bis(dimethylamino)naphthalene / CH₂Cl₂ / 1.) -78 deg C; 2.) room temp., 45 h

With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; palladium dichloride; In dichloromethane; acetic acid;
DOI:10.1021/jo00331a026

Reference yield:

: 76927-64-5
N⁴-Benzyl-N¹,N⁸-bis<2,3-(methylenedioxy)benzoyl>spermidine hydrochloride

: 76927-63-4
N⁴--N¹,N⁸-bis<2,3-(methylenedioxy)benzoyl>spermidine

Guidance literature:: Multi-step reaction with 2 steps

1: PdCl₂ / acetic acid / Ambient temperature

2: 1,8-Bis(dimethylamino)naphthalene / CH₂Cl₂ / 1.) -78 deg C; 2.) room temp., 45 h

With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; palladium dichloride; In dichloromethane; acetic acid;
DOI:10.1021/jo00331a026

Reference yield:

: 73038-05-8
N-(3-aminobutyl)-N-(3-aminopropyl)(phenylmethyl)amine

: 76927-63-4
N⁴--N¹,N⁸-bis<2,3-(methylenedioxy)benzoyl>spermidine

Guidance literature:: Multi-step reaction with 3 steps

1: 1,8-Bis(dimethylamino)naphthalene / CH₂Cl₂ / 16 h / Ambient temperature

2: PdCl₂ / acetic acid / Ambient temperature

3: 1,8-Bis(dimethylamino)naphthalene / CH₂Cl₂ / 1.) -78 deg C; 2.) room temp., 45 h

With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; palladium dichloride; In dichloromethane; acetic acid;
DOI:10.1021/jo00331a026