trinitrosyltrioxohexakis(trimethylsilylmethyl)(triphenylphosphine)-triangulo-trirhenium

Base Information

• Chemical Name: trinitrosyltrioxohexakis(trimethylsilylmethyl)(triphenylphosphine)-triangulo-trirhenium
• CAS No.: 79829-62-2
• Molecular Formula: C₄₂H₈₁N₃O₆PRe₃Si₆
• Molecular Weight: 1482.23
• Mol file: 79829-62-2.mol

Synonyms:

Chemical Property of trinitrosyltrioxohexakis(trimethylsilylmethyl)(triphenylphosphine)-triangulo-trirhenium

Chemical Property:

Purity/Quality:

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Technology Process of trinitrosyltrioxohexakis(trimethylsilylmethyl)(triphenylphosphine)-triangulo-trirhenium

There total 1 articles about trinitrosyltrioxohexakis(trimethylsilylmethyl)(triphenylphosphine)-triangulo-trirhenium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

(η2-nitrosotrimethylsilylmethane)nitrosyloxobis(trimethylsilylmethyl)rhenium (79846-02-9) + triphenylphosphine (603-35-0) → trinitrosyltrioxohexakis(trimethylsilylmethyl)(triphenylphosphine)-triangulo-trirhenium (79829-62-2)

Guidance literature:

In tetrahydrofuran; stirring for 16 h; the soln. evapd, the solid washed with diethyl ether, the residue recrystd. from THF at -30°C; elem. anal.;

DOI:10.1039/DT9810001898

upstream raw materials:

(η2-nitrosotrimethylsilylmethane)nitrosyloxobis(trimethylsilylmethyl)rhenium

triphenylphosphine