Pd(PEtPh2)2(η2-carbon disulfide)

Base Information

Chemical Name:Pd(PEtPh2)2(η2-carbon disulfide)
CAS No.:81191-60-8
Molecular Formula:C₂₉H₃₀P₂PdS₂
Molecular Weight:611.057
Hs Code.:

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Chemical Property of Pd(PEtPh2)2(η2-carbon disulfide)

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Technology Process of Pd(PEtPh2)2(η2-carbon disulfide)

There total 1 articles about Pd(PEtPh2)2(η2-carbon disulfide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 52522-40-4
tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex

: 607-01-2
ethyl-diphenyl-phosphane

: 81191-60-8
Pd(PEtPh2)2(η2-carbon disulfide)

Guidance literature:: With carbon disulfide; In diethyl ether; byproducts: CHCl3, dibenzylideneacetone; to a suspension of Pd-complex in Et2O were added ligand and CS2, stirred at room temp. for 15 min; filtered, washed with Et2O, dried in a N2 stream and in vac.; elem. anal.;

Reference yield: 92.0%

: 81191-60-8
(ethyldiphenylphosphine)2(η2-CS2)palladium

: 607-01-2
ethyl-diphenyl-phosphane

: (ethyldiphenylphosphine)2(dithiocarbonato)palladium(II)*dichloromethane

: (ethyldiphenylphosphine)2(dithiocarbonato)palladium(II)*dichloromethane

Guidance literature:: With O₂; In carbon disulfide; benzene; addn. of CS2 to a soln. of the Pd-compd. in benzene, O2 is bubbled through for 12 h, addn. of 0.5 mmol of the phosphine; most of the solvent is evapd., addn. of ether, the resulting ppt. is filtered off and washed twice with two portions of ether, recrystn. from CH2Cl2/ether; elem. anal.;

Reference yield: 45.0%

: 10544-50-0
sulfur

: 81191-60-8
(ethyldiphenylphosphine)2(η2-CS2)palladium

: 607-01-2
ethyl-diphenyl-phosphane

: 86802-33-7
Pd(PEtPh₂)(trithiocarbonato)

Guidance literature:: In carbon disulfide; benzene; addn. of S8 to a soln. of the Pd-compd. in benzene and CS2, after 5 minstirring addn. of the phosphine and stirring is continued for 48-72 h; the soln. is evapd. to dryness, the residue is extd. with CH2Cl2, crystn. by partial evapn. and addn. of EtOH, washing with EtOH; elem. anal.;