cyclo--MeIle-MeIle-Gly-MeVal-Tyr(Me)-S-Hypr>

Base Information

Chemical Name:cyclo--MeIle-MeIle-Gly-MeVal-Tyr(Me)-S-Hypr>
CAS No.:159170-94-2
Molecular Formula:C₆₈H₁₁₆N₁₀O₁₄Si
Molecular Weight:1325.81
Hs Code.:

cyclo-<Pec-MeVal-Val-MeAsp<β-(valinol tert-butyldimethylsilyl ether)amide>-MeIle-MeIle-Gly-MeVal-Tyr(Me)-S-Hypr>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyclo--MeIle-MeIle-Gly-MeVal-Tyr(Me)-S-Hypr>

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Technology Process of cyclo--MeIle-MeIle-Gly-MeVal-Tyr(Me)-S-Hypr>

There total 4 articles about cyclo--MeIle-MeIle-Gly-MeVal-Tyr(Me)-S-Hypr> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₈H₁₁₈N₁₀O₁₅Si

: 159170-94-2
cyclo--MeIle-MeIle-Gly-MeVal-Tyr(Me)-S-Hypr>

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In toluene; for 20h; Yield given;
DOI:10.1021/jm00039a003

Reference yield:

: 102720-25-2
(S)-1-((tert-butyldimethylsilyl)oxy)-3-methylbutan-2-amine

: 159170-94-2
cyclo--MeIle-MeIle-Gly-MeVal-Tyr(Me)-S-Hypr>

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / (chloromethylene)dimethylammonium chloride, pyridine / acetonitrile / 20 h / -20 °C

2: LiOH / tetrahydrofuran; H₂O / 18 h

3: DEAD, PPh₃ / toluene / 20 h

With pyridine; lithium hydroxide; Vilsmeier reagent; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; water; toluene; acetonitrile;
DOI:10.1021/jm00039a003

Reference yield:

: 159404-79-2
cyclo-

: 159170-94-2
cyclo--MeIle-MeIle-Gly-MeVal-Tyr(Me)-S-Hypr>

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / (chloromethylene)dimethylammonium chloride, pyridine / acetonitrile / 20 h / -20 °C

2: LiOH / tetrahydrofuran; H₂O / 18 h

3: DEAD, PPh₃ / toluene / 20 h

With pyridine; lithium hydroxide; Vilsmeier reagent; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; water; toluene; acetonitrile;
DOI:10.1021/jm00039a003