[2,6-[(2,4,6-Me₃C₆H₂)N=CMe]2C₅H₃N]MnBr₂

Base Information

• Chemical Name: [2,6-[(2,4,6-Me₃C₆H₂)N=CMe]2C₅H₃N]MnBr₂
• CAS No.: 525558-10-5
• Molecular Formula: C₂₇H₃₁Br₂MnN₃
• Molecular Weight: 612.309
• Mol file: 525558-10-5.mol

Synonyms:

Chemical Property of [2,6-[(2,4,6-Me₃C₆H₂)N=CMe]2C₅H₃N]MnBr₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [2,6-[(2,4,6-Me₃C₆H₂)N=CMe]2C₅H₃N]MnBr₂

There total 1 articles about [2,6-[(2,4,6-Me₃C₆H₂)N=CMe]2C₅H₃N]MnBr₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

manganese(II) bromide (13446-03-2) + 2,6-bis[1-(2,4,6-trimethylimino)ethyl]pyridine (210155-39-8) → [2,6-[(2,4,6-Me3C6H2)N=CMe]2C5H3N]MnBr2 (525558-10-5)

Guidance literature:

In acetonitrile; under N2 atm. using Schlenk techniques; org. ligand and MnBr2 heated at reflux in MeCN for 12 h; filtered; crystals were obtained on prolonged standing at ambient temp.;elem. anal.;

DOI:10.1039/b207384f

upstream raw materials:

manganese(II) bromide

2,6-bis[1-(2,4,6-trimethylimino)ethyl]pyridine