Technology Process of C16H16Cl2N2O2S
There total 7 articles about C16H16Cl2N2O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-chlorobenzotriazole;
In
tetrahydrofuran;
DOI:10.1021/jm960673l
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1.) NaH / 1.) DMF, 30 min, 2.) DMF, 90 deg C, 40 min
2: 4 h / 290 °C
3: 72 percent / aq. KOH / methanol / 3 h / Heating
4: SO2Cl2, AcOH / toluene
5: diethyl ether / 2 h / Ambient temperature
6: diethyl ether / Ambient temperature
7: N-chlorobenzotriazole / tetrahydrofuran
With
potassium hydroxide; sulfuryl dichloride; sodium hydride; acetic acid; N-chlorobenzotriazole;
In
tetrahydrofuran; methanol; diethyl ether; toluene;
DOI:10.1021/jm960673l
- Guidance literature:
-
Multi-step reaction with 4 steps
1: SO2Cl2, AcOH / toluene
2: diethyl ether / 2 h / Ambient temperature
3: diethyl ether / Ambient temperature
4: N-chlorobenzotriazole / tetrahydrofuran
With
sulfuryl dichloride; acetic acid; N-chlorobenzotriazole;
In
tetrahydrofuran; diethyl ether; toluene;
DOI:10.1021/jm960673l