2-Piperazinecarboxamide, 4-(2-methoxyphenyl)-1-(phenylmethyl)-

Base Information

Chemical Name:2-Piperazinecarboxamide, 4-(2-methoxyphenyl)-1-(phenylmethyl)-
CAS No.:138286-66-5
Molecular Formula:C19H23N3O2
Molecular Weight:325.40500
Hs Code.:
Mol file:138286-66-5.mol

Synonyms:1-Benzyl-4-(2-methoxy-phenyl)-piperazine-2-carboxylic acid amide;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Piperazinecarboxamide, 4-(2-methoxyphenyl)-1-(phenylmethyl)-

Chemical Property:

Boiling Point:534.8±50.0 °C(Predicted)
PSA：58.80000
Density:1.189±0.06 g/cm3(Predicted)
LogP:2.57450

Purity/Quality:

Safty Information:

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Technology Process of 2-Piperazinecarboxamide, 4-(2-methoxyphenyl)-1-(phenylmethyl)-

There total 1 articles about 2-Piperazinecarboxamide, 4-(2-methoxyphenyl)-1-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15102-42-8
2,3-dibromopropionamide

: 135036-31-6
N-(2-methoxyphenyl)-N'-(phenylmethyl)-1,2-ethanediamine

: 138286-66-5
4-(2-methoxyphenyl)-1-(phenylmethyl)-2-piperazinecarboxamide

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 110 ℃; for 17h;
DOI:10.1021/jm00082a016

Reference yield:

: 138286-66-5
4-(2-methoxyphenyl)-1-(phenylmethyl)-2-piperazinecarboxamide

: 138286-70-1
N-[[4-(2-Methoxyphenyl)piperazin-2-yl]methyl]-4-[(methylsulfonyl)amino]benzamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminum hydride / tetrahydrofuran / 16 h / Heating

2: tetrahydrofuran / 48 h

3: H₂ / Pd(OH)2 / methanol / 48 h / 2585.7 Torr

With lithium aluminium tetrahydride; hydrogen; palladium dihydroxide; In tetrahydrofuran; methanol;
DOI:10.1021/jm00082a016