N'-<7-<5-O--2-deoxy-β-D-erythro-pentofuranosyl>-6,7-dihydro-6-oxo-1H-purin-2-yl>-N,N-dimethylethanimidamide

Base Information

Chemical Name:N'-<7-<5-O--2-deoxy-β-D-erythro-pentofuranosyl>-6,7-dihydro-6-oxo-1H-purin-2-yl>-N,N-dimethylethanimidamide
CAS No.:220252-93-7
Molecular Formula:C₃₅H₃₈N₆O₆
Molecular Weight:638.723
Hs Code.:

N'-<7-<5-O-<bis(4-methoxyphenyl)phenylmethyl>-2-deoxy-β-D-erythro-pentofuranosyl>-6,7-dihydro-6-oxo-1H-purin-2-yl>-N,N-dimethylethanimidamide

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Chemical Property of N'-<7-<5-O--2-deoxy-β-D-erythro-pentofuranosyl>-6,7-dihydro-6-oxo-1H-purin-2-yl>-N,N-dimethylethanimidamide

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Technology Process of N'-<7-<5-O--2-deoxy-β-D-erythro-pentofuranosyl>-6,7-dihydro-6-oxo-1H-purin-2-yl>-N,N-dimethylethanimidamide

There total 2 articles about N'-<7-<5-O--2-deoxy-β-D-erythro-pentofuranosyl>-6,7-dihydro-6-oxo-1H-purin-2-yl>-N,N-dimethylethanimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 220252-92-6
N'-<7-<2-deoxy-β-D-erythro-pentofuranosyl>-6,7-dihydro-6-oxo-1H-purin-2-yl>-N,N-dimethylethanimidamid

: 220252-93-7
N'-<7-<5-O--2-deoxy-β-D-erythro-pentofuranosyl>-6,7-dihydro-6-oxo-1H-purin-2-yl>-N,N-dimethylethanimidamide

Guidance literature:: With dmap; In pyridine; for 5h;
DOI:10.1002/(SICI)1522-2675(19981216)81:12<2244::AID-HLCA2244>3.0.CO;2-I

Reference yield:

: 159791-63-6
7-(2-deoxy-β-D-erythro-pentofuranosyl)-1,7-dihydro-6H-purin-6-one

: 220252-93-7
N'-<7-<5-O--2-deoxy-β-D-erythro-pentofuranosyl>-6,7-dihydro-6-oxo-1H-purin-2-yl>-N,N-dimethylethanimidamide

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / dimethylformamide / 18 h / Ambient temperature

2: 62 percent / 4-(dimethylamino)pyridine / pyridine / 5 h

With dmap; In pyridine; N,N-dimethyl-formamide;
DOI:10.1002/(SICI)1522-2675(19981216)81:12<2244::AID-HLCA2244>3.0.CO;2-I

Reference yield: 65.0%

: 124482-92-4,89992-70-1
2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

: 220252-93-7
N'-<7-<5-O--2-deoxy-β-D-erythro-pentofuranosyl>-6,7-dihydro-6-oxo-1H-purin-2-yl>-N,N-dimethylethanimidamide

: N'-<7-<5-O--2-deoxy-β-D-erythro-pentofuranosyl>-6,7-dihydro-6-oxo-1H-purin-2-yl>-N,N-dimethylethanimidamide 3'-<(2-cyanoethyl)diisopropylphosphoramidite>

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 0.5h; Ambient temperature;
DOI:10.1002/(SICI)1522-2675(19981216)81:12<2244::AID-HLCA2244>3.0.CO;2-I