8-{4-[2-(4'-allyloxybiphenyl-4-yloxy)ethoxy]-2,6-dimethylphenyl}-2-(5-{4-[2-(4'-allyloxybiphenyl-4-yloxy)ethoxy]-2,6-dimethylphenyl}pyridin-2-yl)-[1,10]-phenanthroline

Base Information

Chemical Name:8-{4-[2-(4'-allyloxybiphenyl-4-yloxy)ethoxy]-2,6-dimethylphenyl}-2-(5-{4-[2-(4'-allyloxybiphenyl-4-yloxy)ethoxy]-2,6-dimethylphenyl}pyridin-2-yl)-[1,10]-phenanthroline
CAS No.:866320-99-2
Molecular Formula:C₆₇H₅₉N₃O₆
Molecular Weight:1002.22
Hs Code.:

8-{4-[2-(4'-allyloxybiphenyl-4-yloxy)ethoxy]-2,6-dimethylphenyl}-2-(5-{4-[2-(4'-allyloxybiphenyl-4-yloxy)ethoxy]-2,6-dimethylphenyl}pyridin-2-yl)-[1,10]-phenanthroline

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Chemical Property of 8-{4-[2-(4'-allyloxybiphenyl-4-yloxy)ethoxy]-2,6-dimethylphenyl}-2-(5-{4-[2-(4'-allyloxybiphenyl-4-yloxy)ethoxy]-2,6-dimethylphenyl}pyridin-2-yl)-[1,10]-phenanthroline

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Technology Process of 8-{4-[2-(4'-allyloxybiphenyl-4-yloxy)ethoxy]-2,6-dimethylphenyl}-2-(5-{4-[2-(4'-allyloxybiphenyl-4-yloxy)ethoxy]-2,6-dimethylphenyl}pyridin-2-yl)-[1,10]-phenanthroline

There total 3 articles about 8-{4-[2-(4'-allyloxybiphenyl-4-yloxy)ethoxy]-2,6-dimethylphenyl}-2-(5-{4-[2-(4'-allyloxybiphenyl-4-yloxy)ethoxy]-2,6-dimethylphenyl}pyridin-2-yl)-[1,10]-phenanthroline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 97344-30-4
4-allyloxy-4′-hydroxybiphenyl

: 866320-99-2
8-{4-[2-(4'-allyloxybiphenyl-4-yloxy)ethoxy]-2,6-dimethylphenyl}-2-(5-{4-[2-(4'-allyloxybiphenyl-4-yloxy)ethoxy]-2,6-dimethylphenyl}pyridin-2-yl)-[1,10]-phenanthroline

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / tetrahydrofuran / 1 h / 0 - 20 °C

1.2: 47 percent / tetrahydrofuran / 15 h / Heating

2.1: 92 percent / Cs₂CO₃ / dimethylformamide / 12 h / 80 °C

With sodium hydride; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/b506101f

Reference yield:

: 92-88-6
4,4'-Dihydroxybiphenyl

: 866320-99-2
8-{4-[2-(4'-allyloxybiphenyl-4-yloxy)ethoxy]-2,6-dimethylphenyl}-2-(5-{4-[2-(4'-allyloxybiphenyl-4-yloxy)ethoxy]-2,6-dimethylphenyl}pyridin-2-yl)-[1,10]-phenanthroline

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / tetrahydrofuran / 1 h / 0 - 20 °C

1.2: 66 percent / tetrahydrofuran / 12 h / Heating

2.1: NaH / tetrahydrofuran / 1 h / 0 - 20 °C

2.2: 47 percent / tetrahydrofuran / 15 h / Heating

3.1: 92 percent / Cs₂CO₃ / dimethylformamide / 12 h / 80 °C

With sodium hydride; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/b506101f

Reference yield:

: 338989-85-8
8-(4-methoxy-2,6-dimethyl-phenyl)-9-[5-(4-methoxy-2,6-dimethyl-phenyl)-pyridin-2-yl]-1,10-phenanthroline

: 866320-99-2
8-{4-[2-(4'-allyloxybiphenyl-4-yloxy)ethoxy]-2,6-dimethylphenyl}-2-(5-{4-[2-(4'-allyloxybiphenyl-4-yloxy)ethoxy]-2,6-dimethylphenyl}pyridin-2-yl)-[1,10]-phenanthroline

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / pyridine hydrochloride / 4 h / 185 °C

2: 92 percent / Cs₂CO₃ / dimethylformamide / 12 h / 80 °C

With pyridine hydrochloride; caesium carbonate; In N,N-dimethyl-formamide;
DOI:10.1039/b506101f