Technology Process of 2-(2-azidophenyl)-1-methylbenzimidazole
There total 6 articles about 2-(2-azidophenyl)-1-methylbenzimidazole which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 72 percent / reduced iron, ammonium chloride / propan-1-ol / 3 h / Heating
2: 99.5 percent / methanol / 1 h / Heating
3: 71 percent / alumina / toluene
4: 87 percent / reduced iron, ammonium chloride
5: 1.) sodium nitrite, conc. hydrochloric acid, 2.) sodium azide / 1.) water, 0 deg C, 2.) sodium acetate in water
With
hydrogenchloride; aluminum oxide; sodium azide; ammonium chloride; iron; sodium nitrite;
In
methanol; propan-1-ol; toluene;
DOI:10.1039/P19800002387
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 91 percent / potassium carbonate, water / pyridine / 10 h / Heating
2: 72 percent / reduced iron, ammonium chloride / propan-1-ol / 3 h / Heating
3: 99.5 percent / methanol / 1 h / Heating
4: 71 percent / alumina / toluene
5: 87 percent / reduced iron, ammonium chloride
6: 1.) sodium nitrite, conc. hydrochloric acid, 2.) sodium azide / 1.) water, 0 deg C, 2.) sodium acetate in water
With
hydrogenchloride; aluminum oxide; sodium azide; ammonium chloride; water; iron; potassium carbonate; sodium nitrite;
In
pyridine; methanol; propan-1-ol; toluene;
DOI:10.1039/P19800002387
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 99.5 percent / methanol / 1 h / Heating
2: 71 percent / alumina / toluene
3: 87 percent / reduced iron, ammonium chloride
4: 1.) sodium nitrite, conc. hydrochloric acid, 2.) sodium azide / 1.) water, 0 deg C, 2.) sodium acetate in water
With
hydrogenchloride; aluminum oxide; sodium azide; ammonium chloride; iron; sodium nitrite;
In
methanol; toluene;
DOI:10.1039/P19800002387
