5-Acetamido-4,8-anhydro-7,9-O-benzylidene-1,2-O-cyclohexylidene-5-deoxy-6-C-(methoxymethoxymethyl)-4,7-bis-O-(methoxymethyl)-D-arabino-L-gulo-nonitol

Base Information

Chemical Name:5-Acetamido-4,8-anhydro-7,9-O-benzylidene-1,2-O-cyclohexylidene-5-deoxy-6-C-(methoxymethoxymethyl)-4,7-bis-O-(methoxymethyl)-D-arabino-L-gulo-nonitol
CAS No.:131424-66-3
Molecular Formula:C₃₁H₄₇NO₁₂
Molecular Weight:625.714
Hs Code.:

5-Acetamido-4,8-anhydro-7,9-O-benzylidene-1,2-O-cyclohexylidene-5-deoxy-6-C-(methoxymethoxymethyl)-4,7-bis-O-(methoxymethyl)-D-arabino-L-gulo-nonitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Acetamido-4,8-anhydro-7,9-O-benzylidene-1,2-O-cyclohexylidene-5-deoxy-6-C-(methoxymethoxymethyl)-4,7-bis-O-(methoxymethyl)-D-arabino-L-gulo-nonitol

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Technology Process of 5-Acetamido-4,8-anhydro-7,9-O-benzylidene-1,2-O-cyclohexylidene-5-deoxy-6-C-(methoxymethoxymethyl)-4,7-bis-O-(methoxymethyl)-D-arabino-L-gulo-nonitol

There total 4 articles about 5-Acetamido-4,8-anhydro-7,9-O-benzylidene-1,2-O-cyclohexylidene-5-deoxy-6-C-(methoxymethoxymethyl)-4,7-bis-O-(methoxymethyl)-D-arabino-L-gulo-nonitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 131424-60-7
5-Acetamido-2,6-anhydro-1,3-O-benzylidene-8,9-O-cyclohexylidene-5-deoxy-6-C-(hydroxymethyl)-4,7-bis-O-(methoxymethyl)-D-arabino-L-gulo-nonitol

: 107-30-2
chloromethyl methyl ether

: 131424-66-3
5-Acetamido-4,8-anhydro-7,9-O-benzylidene-1,2-O-cyclohexylidene-5-deoxy-6-C-(methoxymethoxymethyl)-4,7-bis-O-(methoxymethyl)-D-arabino-L-gulo-nonitol

Guidance literature:: With N-ethyl-N,N-diisopropylamine; for 15h; Ambient temperature;
DOI:10.1002/hlca.19900730620

Reference yield:

: 114102-93-1
(4R)-5-acetamido-4,8-anhydro-7,9-O-benzylidene-1,2-O-cyclohexylidene-5-deoxy-4-C-nitro-D-gluco-L-erythro-nonitol

: 131424-66-3
5-Acetamido-4,8-anhydro-7,9-O-benzylidene-1,2-O-cyclohexylidene-5-deoxy-6-C-(methoxymethoxymethyl)-4,7-bis-O-(methoxymethyl)-D-arabino-L-gulo-nonitol

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / Et(iPr)2N / CH₂Cl₂ / 1.) 1 h, 0 deg C, 2.) 48 h, room temperature

2: 1.) NaH / 1.) DMSO, 30 min, 2.) DMSO, hν, 5 h, room temperature

4: 91 percent / Et(iPr)2N / 15 h / Ambient temperature

With sodium hydride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1002/hlca.19900730620

Reference yield:

: 131424-58-3
5-Acetamido-7,9-O-benzylidene-1,2-O-cyclohexylidene-4,5-dideoxy-3,6-bis-O-(methoxymethyl)-4-nitro-D-gluco-L-erythro-nonulopyranose

: 131424-66-3
5-Acetamido-4,8-anhydro-7,9-O-benzylidene-1,2-O-cyclohexylidene-5-deoxy-6-C-(methoxymethoxymethyl)-4,7-bis-O-(methoxymethyl)-D-arabino-L-gulo-nonitol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMSO, 30 min, 2.) DMSO, hν, 5 h, room temperature

3: 91 percent / Et(iPr)2N / 15 h / Ambient temperature

With sodium hydride; N-ethyl-N,N-diisopropylamine;
DOI:10.1002/hlca.19900730620