Propanoic acid, 2-(4-methylphenoxy)-, (2S)-

Base Information

Chemical Name:Propanoic acid, 2-(4-methylphenoxy)-, (2S)-
CAS No.:13832-02-5
Molecular Formula:C10H12O3
Molecular Weight:180.203
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Propanoic acid, 2-(4-methylphenoxy)-, (2S)-

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Technology Process of Propanoic acid, 2-(4-methylphenoxy)-, (2S)-

There total 9 articles about Propanoic acid, 2-(4-methylphenoxy)-, (2S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 106-44-5
p-cresol

: 32644-15-8,10327-08-9
(S)-2-bromopropanoic acid

: 13832-02-5
(S)-2-(4-methylphenoxy)propanoic acid

Guidance literature:: p-cresol; (S)-2-bromopropanoic acid; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 5h;

With sodium hydroxide; In tetrahydrofuran; mineral oil; at 20 ℃; for 1h;

With hydrogenchloride; In tetrahydrofuran; water; mineral oil; pH=1;

Reference yield:

: 22504-83-2
2-(4-methylphenoxy)propanoic acid

: 14013-55-9
(R)-2-(4-methylphenoxy)propanoic acid

: 13832-02-5
(S)-2-(4-methylphenoxy)propanoic acid

Guidance literature:: With Nocardia diaphanozonaria cells; glycerol; peptone; beef extract; yeast extract; In water; at 30 ℃; for 48h; pH=7.0; Title compound not separated from byproducts;
DOI:10.1021/jo034253x

Reference yield:

: 106-44-5
p-cresol

: 13832-02-5
(S)-2-(4-methylphenoxy)propanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 26 percent / sodium hydride / tetrahydrofuran / 14 h / 20 °C

2: 94 percent / potassium hydroxide / ethanol; H₂O / 4 h / 0 °C

3: Nocardia diaphanozonaria cells; glycerol; peptone / beef extract; yeast extract / H₂O / 48 h / 30 °C / pH 7.0

With potassium hydroxide; Nocardia diaphanozonaria cells; sodium hydride; glycerol; peptone; beef extract; yeast extract; In tetrahydrofuran; ethanol; water;
DOI:10.1021/jo034253x