trans-cinnamic acid-[2]naphthylmethyl ester

Base Information

• Chemical Name: trans-cinnamic acid-[2]naphthylmethyl ester
• CAS No.: 102001-58-1
• Molecular Formula: C₂₀H₁₆O₂
• Molecular Weight: 288.346
• Mol file: 102001-58-1.mol

Synonyms:

Chemical Property of trans-cinnamic acid-[2]naphthylmethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trans-cinnamic acid-[2]naphthylmethyl ester

There total 2 articles about trans-cinnamic acid-[2]naphthylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(p-hydroxyphenyl)boronic acid (71597-85-8) + benzenediazonium tetrafluoroborate (369-57-3) + 2-propenoic acid 2-naphthalenylmethyl ester (93359-80-9) → 2-naphthylmethyl 3-(4-hydroxyphenyl)-3-phenylpropanoate + 2-naphthylmethyl 3-(4-hydroxyphenyl)-3-phenylpropanoate + trans-cinnamic acid-[2]naphthylmethyl ester (102001-58-1)

Guidance literature:

(p-hydroxyphenyl)boronic acid; benzenediazonium tetrafluoroborate; With (R)-3,3'-bis(9-anthracenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium hydrogencarbonate; In diethyl ether; for 0.0833333h; Inert atmosphere; Schlenk technique;

2-propenoic acid 2-naphthalenylmethyl ester; In diethyl ether; at 20 ℃; for 20h; Reagent/catalyst; enantioselective reaction; Inert atmosphere; Schlenk technique;

DOI:10.1021/jacs.7b06917

Reference yield:

→ trans-cinnamic acid-[2]naphthylmethyl ester (102001-58-1)

Guidance literature:

/BRN= 3142183/;

upstream raw materials:

(p-hydroxyphenyl)boronic acid

benzenediazonium tetrafluoroborate

2-propenoic acid 2-naphthalenylmethyl ester