Sulfamic acid, (2-phenylethyl)-

Base Information

• Chemical Name: Sulfamic acid, (2-phenylethyl)-
• CAS No.: 138337-13-0
• Molecular Formula: C8H11NO3S
• Molecular Weight: 201.246
• Mol file: 138337-13-0.mol

Synonyms:

Chemical Property of Sulfamic acid, (2-phenylethyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Sulfamic acid, (2-phenylethyl)-

There total 1 articles about Sulfamic acid, (2-phenylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

phenethylamine (64-04-0) → N-(2-phenylethyl)sulfamic acid (138337-13-0)

Guidance literature:

With chlorosulfonic acid; In chloroform; for 0.166667h;

DOI:10.1021/jo00030a037

Reference yield: 62.0%

N-(2-phenylethyl)sulfamic acid (138337-13-0) → potassium N-nitroso-N-(2-phenylethyl)sulfamate (138337-15-2)

Guidance literature:

With potassium nitrite; In water; 1) 25 deg C, 1 min, 2) 4 deg C, 20 min;

DOI:10.1021/jo00030a037

Reference yield:

N-(2-phenylethyl)sulfamic acid (138337-13-0) → 2-phenylethylsulfamoyl chloride (223560-62-1)

Guidance literature:

With phosphorus pentachloride; In benzene; for 24h; Heating;

DOI:10.1021/jm980348t

upstream raw materials:

phenethylamine

Downstream raw materials:

potassium N-nitroso-N-(2-phenylethyl)sulfamate

2-phenylethylsulfamoyl chloride

bis(2-phenylethyl) sulfate