C₃₃H₃₅FN₂O₅

Base Information

Chemical Name:C₃₃H₃₅FN₂O₅
CAS No.:1422252-09-2
Molecular Formula:C₃₃H₃₅FN₂O₅
Molecular Weight:558.65
Hs Code.:

C<sub>33</sub>H<sub>35</sub>FN<sub>2</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₃₃H₃₅FN₂O₅

Chemical Property:

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Technology Process of C₃₃H₃₅FN₂O₅

There total 8 articles about C₃₃H₃₅FN₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1422252-09-2
C₃₃H₃₅FN₂O₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 3 h / 20 °C

2.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; trifuran-2-yl-phosphane; potassium phosphate / water; 1,2-dimethoxyethane / Inert atmosphere; Reflux

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium phosphate; trifuran-2-yl-phosphane; sodium hydride; In 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; mineral oil; 2.1: |Suzuki Coupling;
DOI:10.1139/cjc-2012-0319

Reference yield:

: 121219-03-2
4-bromo-3-fluorophenol

: 1422252-09-2
C₃₃H₃₅FN₂O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / dimethyl sulfoxide / 30 h / 120 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.67 h / -78 °C / Inert atmosphere

2.2: 3.5 h / -78 - 20 °C

3.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; trifuran-2-yl-phosphane; potassium phosphate / water; 1,2-dimethoxyethane / Inert atmosphere; Reflux

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium phosphate; n-butyllithium; trifuran-2-yl-phosphane; potassium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; hexane; water; dimethyl sulfoxide; 3.1: |Suzuki Coupling;
DOI:10.1139/cjc-2012-0319

Reference yield:

: 372-48-5
2-fluoropyridine

: 1422252-09-2
C₃₃H₃₅FN₂O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / dimethyl sulfoxide / 30 h / 120 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.67 h / -78 °C / Inert atmosphere

2.2: 3.5 h / -78 - 20 °C

3.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; trifuran-2-yl-phosphane; potassium phosphate / water; 1,2-dimethoxyethane / Inert atmosphere; Reflux

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium phosphate; n-butyllithium; trifuran-2-yl-phosphane; potassium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; hexane; water; dimethyl sulfoxide; 3.1: |Suzuki Coupling;
DOI:10.1139/cjc-2012-0319