Technology Process of 11,11'-<1,4-Phenylenbis(oxy)>bis(undecansaeure)-dimethylester
There total 1 articles about 11,11'-<1,4-Phenylenbis(oxy)>bis(undecansaeure)-dimethylester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium methylate;
In
methanol;
for 10h;
Heating;
-
-
73819-07-5,73837-64-6
15,15-Bis(11,11,11-triphenylundecyl)-2,14,16,28-tetraoxatricyclo<27.2.2.013,17>tritriaconta-1(31),29,32-trien
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 78 percent / sodium sand / xylene / 2 h / 110 °C
2: 81 percent / lithium alanate / diethyl ether / 1 h / Heating
3: 59 percent / p-toluenesulfonic acid, Mg(ClO4)2 / benzene / 24 h / Heating
4: 1.) BuLi / 1.) ether, THF, 15 min, 0 deg C, 15 min, room temp., 2.) 2 h, room temp.
With
lithium aluminium tetrahydride; n-butyllithium; magnesium(II) perchlorate; sodium sand; toluene-4-sulfonic acid;
In
diethyl ether; xylene; benzene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 78 percent / sodium sand / xylene / 2 h / 110 °C
2: 81 percent / lithium alanate / diethyl ether / 1 h / Heating
3: 59 percent / p-toluenesulfonic acid, Mg(ClO4)2 / benzene / 24 h / Heating
4: 85 percent / NaI / acetone / 20 h / Heating
With
lithium aluminium tetrahydride; magnesium(II) perchlorate; sodium sand; toluene-4-sulfonic acid; sodium iodide;
In
diethyl ether; acetone; xylene; benzene;