p-cyanobenzoylferrocene

Base Information

Chemical Name:p-cyanobenzoylferrocene
CAS No.:84206-50-8
Molecular Formula:C₁₈H₁₃FeNO
Molecular Weight:315.154
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-cyanobenzoylferrocene

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Technology Process of p-cyanobenzoylferrocene

There total 1 articles about p-cyanobenzoylferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 102-54-5,55404-68-7
ferrocene

: 6068-72-0
4-cyanobenzoyl chlorIde

: 84206-50-8
p-cyanobenzoylferrocene

Guidance literature:: With aluminium trichloride; In carbon disulfide; dissolution of p-cyanobenzoyl chloride and anhyd. AlCl3 in CS2, adding during 30 min to a warm soln. of ferrocene in CS2 with stirring; hydrolyzing by ice-cooled dilute HCl after 20 h, extn. with ether, washing etheral extract with water, aq. NaOH and water, drying over anhyd. Na2SO4, slow evapn. of ether, recrystn. from n-hexane, elem. anal.;

Reference yield: 85.0%

: 16940-66-2
sodium tetrahydroborate

: 84206-50-8
p-cyanobenzoylferrocene

: 84206-46-2
(C₅H₅)Fe(C₅H₄CH(C₆H₄CN)OH)

Guidance literature:: In methanol; Fe complex dissolved in MeOH, excess of NaBH4 added; addn. of ice water, recrystn. (MeOH); elem. anal.;
DOI:10.1016/S0022-328X(00)87079-5