((C₆H₅)3P)2N⁽¹⁺⁾*S₄N₅O^(1-)=(((C₆H₅)3P)2N)S₄N₅O

Base Information

• Chemical Name: ((C₆H₅)3P)2N⁽¹⁺⁾*S₄N₅O^(1-)=(((C₆H₅)3P)2N)S₄N₅O
• CAS No.: 86163-11-3
• Molecular Formula: C₃₆H₃₀NP₂*N₅OS₄
• Molecular Weight: 752.885

Synonyms:

Chemical Property of ((C₆H₅)3P)2N⁽¹⁺⁾*S₄N₅O^(1-)=(((C₆H₅)3P)2N)S₄N₅O

Chemical Property:

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Technology Process of ((C₆H₅)3P)2N⁽¹⁺⁾*S₄N₅O^(1-)=(((C₆H₅)3P)2N)S₄N₅O

There total 2 articles about ((C₆H₅)3P)2N⁽¹⁺⁾*S₄N₅O^(1-)=(((C₆H₅)3P)2N)S₄N₅O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

bis(triphenylphosphine)iminium trisulfur trinitride → ((C6H5)3P)2N(1+)*S3N3O(1-)=(((C6H5)3P)2N)S3N3O (81260-54-0) + ((C6H5)3P)2N(1+)*S4N5O(1-)=(((C6H5)3P)2N)S4N5O (86163-11-3) + bis(triphenylphosphine)iminium tetrasulfur pentanitride (72884-88-9)

Guidance literature:

With O₂; In acetonitrile; O2 bubbled into stirred (((C6H5)3P)2N)S3N3 soln. for 30 min, left to stand for 1 h; concd. (vac.), warmed, cooled to -20°C overnight, crystals manually sepd., recrystd. (MeCN); elem. anal.;

Reference yield:

bis(triphenylphosphine)iminium trisulfur trinitride → ((C6H5)3P)2N(1+)*S4N5O(1-)=(((C6H5)3P)2N)S4N5O (86163-11-3) + bis(triphenylphosphine)iminium tetrasulfur pentanitride (72884-88-9) + ((C6H5)3P)2N(1+)*S3N3O2(1-)=(((C6H5)3P)2N)S3N3O2 (86176-90-1)

Guidance literature:

With O₂; In acetonitrile; (((C6H5)3P)2N)S3N3 slurry allowed to react with atm. O2 by slow diffusion for 24 h; concd., cooled to -20°C overnight, filtered, concd. (vac.), cooled to -20°C for 24 h;

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