Natrium-tris(phenylsulfonylimido)chlorsulfonat

Base Information

• Chemical Name: Natrium-tris(phenylsulfonylimido)chlorsulfonat
• CAS No.: 83125-12-6
• Molecular Formula: C₁₈H₁₅ClN₃O₆S₄*Na
• Molecular Weight: 556.04
• Mol file: 83125-12-6.mol

Synonyms:

Chemical Property of Natrium-tris(phenylsulfonylimido)chlorsulfonat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Natrium-tris(phenylsulfonylimido)chlorsulfonat

There total 2 articles about Natrium-tris(phenylsulfonylimido)chlorsulfonat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

Natrium-bis(phenylsulfonylimido)methoxysulfinat (15315-01-2) → Natrium-tris(phenylsulfonylimido)chlorsulfonat (83125-12-6)

Guidance literature:

With chlorine; In dichloromethane; 1) -40 deg C, 2) r.t., 48 h;

Reference yield:

N,N'-bis(phenylsulfonyl)sulfur diimide (667-20-9) → Natrium-tris(phenylsulfonylimido)chlorsulfonat (83125-12-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / acetonitrile / 1) -50 to -40 deg C, 2) r.t., 14 h

2: 32 percent / Cl₂ / CH₂Cl₂ / 1) -40 deg C, 2) r.t., 48 h

With chlorine; In dichloromethane; acetonitrile;

upstream raw materials:

Natrium-bis(phenylsulfonylimido)methoxysulfinat

N,N'-bis(phenylsulfonyl)sulfur diimide