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C30H28N2O3S

Base Information
  • Chemical Name:C30H28N2O3S
  • CAS No.:99657-04-2
  • Molecular Formula:C30H28N2O3S
  • Molecular Weight:496.63
  • Hs Code.:
C<sub>30</sub>H<sub>28</sub>N<sub>2</sub>O<sub>3</sub>S

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Chemical Property of C30H28N2O3S
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Technology Process of C30H28N2O3S

There total 9 articles about C30H28N2O3S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With trifluoroacetic anhydride; In toluene; 0 deg C then reflux;
DOI:10.1021/ja00215a039
Guidance literature:
With trifluoroacetic anhydride; bis-[(trifluoroacetoxy)iodo]benzene; In toluene; Heating;
DOI:10.1021/ja00215a039
Guidance literature:
Multi-step reaction with 5 steps
1: 76 percent / benzyltrimethylammonium chloride, 30percent aq. sodium hydroxyde / CH2Cl2 / 1 h / 0 °C
2: 4 Angstroem molecular sieves / tetrahydrofuran / 16 h
3: 67 percent / toluene / 0.5 h room temperature then 3 h reflux
4: m-chloroperbenzoic acid, 10percent aq. sodium bicarbonate / CH2Cl2 / 1 h / 0 °C
5: 1.) trifluoroacetic anhydride / 1.) CH2Cl2, 1 h, room temperature, 2.) toluene, 1 h, reflux
With sodium hydroxide; 4 A molecular sieve; benzyltrimethylammonium chloride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ja00262a006
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