trans-{Rh(1,3:4,6-bis(1,4-(4-(3-pyridyl)-1-oxabutyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H)-dione)Cl₂}Cl*4H₂O*CH₃OH

Base Information

• Chemical Name: trans-{Rh(1,3:4,6-bis(1,4-(4-(3-pyridyl)-1-oxabutyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H)-dione)Cl₂}Cl*4H₂O*CH₃OH
• CAS No.: 118715-80-3
• Molecular Formula: CH₄O*C₆₄H₆₂Cl₂N₈O₆Rh*Cl*4H₂O
• Molecular Weight: 1352.61

Synonyms:

Chemical Property of trans-{Rh(1,3:4,6-bis(1,4-(4-(3-pyridyl)-1-oxabutyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H)-dione)Cl₂}Cl*4H₂O*CH₃OH

Chemical Property:

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Technology Process of trans-{Rh(1,3:4,6-bis(1,4-(4-(3-pyridyl)-1-oxabutyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H)-dione)Cl₂}Cl*4H₂O*CH₃OH

There total 1 articles about trans-{Rh(1,3:4,6-bis(1,4-(4-(3-pyridyl)-1-oxabutyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H)-dione)Cl₂}Cl*4H₂O*CH₃OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

rhodium(III) chloride trihydrate + 1,3:4,6-bis(1,4-(4-(3-pyridyl)-1-oxabutyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H,4H,6H)-dione (118715-71-2) → trans-{Rh(1,3:4,6-bis(1,4-(4-(3-pyridyl)-1-oxabutyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H)-dione)Cl2}Cl*4H2O*CH3OH (118715-80-3)

Guidance literature:

In methanol; 16 h at reflux temperature; filtration, evapd. in vac., elem. anal;

DOI:10.1021/ja00188a022

upstream raw materials:

1,3:4,6-bis(1,4-(4-(3-pyridyl)-1-oxabutyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H,4H,6H)-dione

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