[Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COOMe)(COCH₂Cl)-P,P')]PF₆

Base Information

Chemical Name:[Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COOMe)(COCH₂Cl)-P,P')]PF₆
CAS No.:494831-30-0
Molecular Formula:C₄₆H₄₉ClNO₅P₂Pd*F₆P
Molecular Weight:1044.68
Hs Code.:

[Pd(2,3-(MeO)2C<sub>6</sub>H<sub>2</sub>CH=N(Cy)-C<sub>6</sub>,N)((Ph<sub>2</sub>P)2CHCH<sub>2</sub>CH(COOMe)(COCH<sub>2</sub>Cl)-P,P')]PF<sub>6</sub>

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Chemical Property of [Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COOMe)(COCH₂Cl)-P,P')]PF₆

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Technology Process of [Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COOMe)(COCH₂Cl)-P,P')]PF₆

There total 1 articles about [Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COOMe)(COCH₂Cl)-P,P')]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 32807-28-6,935731-94-5
Methyl 4-chloroacetoacetate

: 494831-09-3
[Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CCH₂-P,P')]PF₆

: 494831-30-0
[Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COOMe)(COCH₂Cl)-P,P')]PF₆

Guidance literature:: sodium carbonate; In chloroform; under Ar, 2 equiv. of the ester, heating in dry CHCl3 at 45 °C for 4 h in the presence of anhyd. Na2CO3; soln. was cooled to room temp., filtered through Celite, evapd. in vac.,residue was triturated with Et2O, filtered off, washed with cold Et2O, dried in vac.;
DOI:10.1039/b203864a