α-lithium methylenediphenylphosphine borane

Base Information

Chemical Name:α-lithium methylenediphenylphosphine borane
CAS No.:452969-86-7
Molecular Formula:BH₃*C₁₃H₁₂LiP
Molecular Weight:219.988
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-lithium methylenediphenylphosphine borane

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Technology Process of α-lithium methylenediphenylphosphine borane

There total 2 articles about α-lithium methylenediphenylphosphine borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 598-30-1
sec.-butyllithium

: methyldiphenylphosphine borane complex

: 452969-86-7
α-lithium methylenediphenylphosphine borane

Guidance literature:: In tetrahydrofuran; BuLi adding into THF soln. of phosphine borane at -78°C, according to Imamoto et al. J. Am. Chem. Soc. 112 (1990) 5244;
DOI:10.1016/0020-1693(95)90063-C

Reference yield:

: 1486-28-8
diphenyl(methyl)phosphine

: 452969-86-7
α-lithium methylenediphenylphosphine borane

Guidance literature:: Multi-step reaction with 2 steps

1: toluene

2: tetrahydrofuran

In tetrahydrofuran; toluene;
DOI:10.1016/0020-1693(95)90063-C