decamethylnickelocenium hydrogen-7,7,8,8-tetracyanoperfluoro-p-quinodimethandiide

Base Information

• Chemical Name: decamethylnickelocenium hydrogen-7,7,8,8-tetracyanoperfluoro-p-quinodimethandiide
• CAS No.: 182244-45-7
• Molecular Formula: C₁₂HF₄N₄*C₂₀H₃₀Ni
• Molecular Weight: 606.309
• Mol file: 182244-45-7.mol

Synonyms:

Chemical Property of decamethylnickelocenium hydrogen-7,7,8,8-tetracyanoperfluoro-p-quinodimethandiide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of decamethylnickelocenium hydrogen-7,7,8,8-tetracyanoperfluoro-p-quinodimethandiide

There total 1 articles about decamethylnickelocenium hydrogen-7,7,8,8-tetracyanoperfluoro-p-quinodimethandiide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

bis(pentamethylcyclopentadienyl)nickel + 2,3,5,6-tetrafluoro-7,7',8,8'-tetracyanoquinodimethane (29261-33-4) → decamethylnickelocenium hydrogen-7,7,8,8-tetracyanoperfluoro-p-quinodimethandiide (182244-45-7) + decamethylnickelocenium 7,7,8,8-tetracyanoperfluoro-p-quinodimethandiide

Guidance literature:

In tetrahydrofuran; recrystn. (MeCN), the byproduct being isolated from the concd. mother-liquor after cooling to -40°C for several d;

DOI:10.1039/cc9960001979

upstream raw materials:

2,3,5,6-tetrafluoro-7,7',8,8'-tetracyanoquinodimethane