(Xyl-N=)Cl₃W(CH₂CH₂C(=O)OEt)

Base Information

Chemical Name:(Xyl-N=)Cl₃W(CH₂CH₂C(=O)OEt)
CAS No.:900159-19-5
Molecular Formula:C₁₃H₁₈Cl₃NO₂W
Molecular Weight:510.5
Hs Code.:

(Xyl-N=)Cl<sub>3</sub>W(CH<sub>2</sub>CH<sub>2</sub>C(=O)OEt)

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Chemical Property of (Xyl-N=)Cl₃W(CH₂CH₂C(=O)OEt)

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Technology Process of (Xyl-N=)Cl₃W(CH₂CH₂C(=O)OEt)

There total 1 articles about (Xyl-N=)Cl₃W(CH₂CH₂C(=O)OEt) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 900159-27-5
[Et₄N][(Xyl-N=)WCl₅]

: 911641-23-1
bis(2-carboethoxyethyl)zinc

: 900159-19-5
(Xyl-N=)Cl₃W(CH₂CH₂C(=O)OEt)

Guidance literature:: In diethyl ether; under Ar atm. to suspn. (Et4N)((Xyl-N=)WCl5) in ether at -78°C was added soln. Zn(CH2CH2CO2Et) in ether, allowed to warm to room temp. and stirred for 2 h; volatiles were removed, residue was extd. by hexane, extract was concd.;elem. anal.;
DOI:10.1021/om060264f

Reference yield: 57.0%

: 900159-19-5
(Xyl-N=)Cl₃W(CH₂CH₂C(=O)OEt)

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 108-88-3,15644-74-3,16713-13-6
toluene

: (Xyl-N=)W(C₉=N-Xyl)CH₂CH₂CO₂Et)(CNXyl)Cl₃*0.33toluene

Guidance literature:: In toluene; under Ar atm. to soln. W complex in toluene was layered soln. 2,6-dimethylphenylisocyanide in toluene, 3 days; ppt. was washed with hexane and dried in vacuo; elem. anal.;
DOI:10.1021/om060264f