N-{(2S,3R,4R,5S,6R)-2-Allyloxy-5-benzyloxy-4-(3-benzyloxy-decyloxy)-6-[(2R,3R,4R,5S,6R)-4,5-dihydroxy-6-hydroxymethyl-3-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxymethyl]-tetrahydro-pyran-3-yl}-2,2,2-trifluoro-acetamide

Base Information

Chemical Name:N-{(2S,3R,4R,5S,6R)-2-Allyloxy-5-benzyloxy-4-(3-benzyloxy-decyloxy)-6-[(2R,3R,4R,5S,6R)-4,5-dihydroxy-6-hydroxymethyl-3-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxymethyl]-tetrahydro-pyran-3-yl}-2,2,2-trifluoro-acetamide
CAS No.:139573-89-0
Molecular Formula:C₄₃H₅₈F₆N₂O₁₂
Molecular Weight:908.93
Hs Code.:

N-{(2S,3R,4R,5S,6R)-2-Allyloxy-5-benzyloxy-4-(3-benzyloxy-decyloxy)-6-[(2R,3R,4R,5S,6R)-4,5-dihydroxy-6-hydroxymethyl-3-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxymethyl]-tetrahydro-pyran-3-yl}-2,2,2-trifluoro-acetamide

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Suppliers and Price of N-{(2S,3R,4R,5S,6R)-2-Allyloxy-5-benzyloxy-4-(3-benzyloxy-decyloxy)-6-[(2R,3R,4R,5S,6R)-4,5-dihydroxy-6-hydroxymethyl-3-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxymethyl]-tetrahydro-pyran-3-yl}-2,2,2-trifluoro-acetamide

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Chemical Property of N-{(2S,3R,4R,5S,6R)-2-Allyloxy-5-benzyloxy-4-(3-benzyloxy-decyloxy)-6-[(2R,3R,4R,5S,6R)-4,5-dihydroxy-6-hydroxymethyl-3-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxymethyl]-tetrahydro-pyran-3-yl}-2,2,2-trifluoro-acetamide

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Technology Process of N-{(2S,3R,4R,5S,6R)-2-Allyloxy-5-benzyloxy-4-(3-benzyloxy-decyloxy)-6-[(2R,3R,4R,5S,6R)-4,5-dihydroxy-6-hydroxymethyl-3-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxymethyl]-tetrahydro-pyran-3-yl}-2,2,2-trifluoro-acetamide

There total 11 articles about N-{(2S,3R,4R,5S,6R)-2-Allyloxy-5-benzyloxy-4-(3-benzyloxy-decyloxy)-6-[(2R,3R,4R,5S,6R)-4,5-dihydroxy-6-hydroxymethyl-3-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxymethyl]-tetrahydro-pyran-3-yl}-2,2,2-trifluoro-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 137014-86-9
allyl 6-O-<(3,4,6-tri-O-acetyl-2-deoxy-2-triflouroacetamido)-β-D-glucopyranosyl>-4-O-benzyl-3-O-<(3RS)-3-(benzyloxy)decanyl>-2-deoxy-2-triflouroacetamido-α-D-glucopyranoside

: 139573-89-0,139629-83-7
N-{(2S,3R,4R,5S,6R)-2-Allyloxy-5-benzyloxy-4-(3-benzyloxy-decyloxy)-6-[(2R,3R,4R,5S,6R)-4,5-dihydroxy-6-hydroxymethyl-3-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxymethyl]-tetrahydro-pyran-3-yl}-2,2,2-trifluoro-acetamide

Guidance literature:: With ammonium hydroxide; In methanol; at 20 - 25 ℃; for 4h;
DOI:10.1016/0008-6215(91)89007-3

Reference yield:

: 7139-63-1
1,3,4,6-tetra-O-acetyl-2-(trifluoroacetamido)-2-deoxy-β-D-glucopyranoside

: 139573-89-0,139629-83-7
N-{(2S,3R,4R,5S,6R)-2-Allyloxy-5-benzyloxy-4-(3-benzyloxy-decyloxy)-6-[(2R,3R,4R,5S,6R)-4,5-dihydroxy-6-hydroxymethyl-3-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxymethyl]-tetrahydro-pyran-3-yl}-2,2,2-trifluoro-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 30percent HBr / acetic acid / 0.08 h / 20 °C

2: 85 percent / anhydr. CaSO₄, Hg(CN)2 / CHCl₃ / 15 h / Heating

3: 42 percent / NH₄OH / methanol / 4 h / 20 - 25 °C

With calcium sulfate; ammonium hydroxide; hydrogen bromide; mercury(II) cyanide; In methanol; chloroform; acetic acid;
DOI:10.1016/0008-6215(91)89007-3

Reference yield:

: 6736-63-6
3,4,6-tri-O-acetyl-2-deoxy-2-trifluoroacetamido-α-D-glucospyranosyl bromide

: 139573-89-0,139629-83-7
N-{(2S,3R,4R,5S,6R)-2-Allyloxy-5-benzyloxy-4-(3-benzyloxy-decyloxy)-6-[(2R,3R,4R,5S,6R)-4,5-dihydroxy-6-hydroxymethyl-3-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxymethyl]-tetrahydro-pyran-3-yl}-2,2,2-trifluoro-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / anhydr. CaSO₄, Hg(CN)2 / CHCl₃ / 15 h / Heating

2: 42 percent / NH₄OH / methanol / 4 h / 20 - 25 °C

With calcium sulfate; ammonium hydroxide; mercury(II) cyanide; In methanol; chloroform;
DOI:10.1016/0008-6215(91)89007-3