tris(dicyclohexylacetamide)tetraisothiocyanatouranium(IV)

Base Information

Chemical Name:tris(dicyclohexylacetamide)tetraisothiocyanatouranium(IV)
CAS No.:93267-70-0
Molecular Formula:C₄₆H₇₅N₇O₃S₄U
Molecular Weight:1140.44
Hs Code.:

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Chemical Property of tris(dicyclohexylacetamide)tetraisothiocyanatouranium(IV)

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Technology Process of tris(dicyclohexylacetamide)tetraisothiocyanatouranium(IV)

There total 2 articles about tris(dicyclohexylacetamide)tetraisothiocyanatouranium(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1563-91-3
N,N-dicyclohexylacetamide

: 10026-10-5
uranium(IV) chloride

: 93267-70-0
tris(dicyclohexylacetamide)tetraisothiocyanatouranium(IV)

Guidance literature:: With potassium thioacyanate; In tetrahydrofuran; addn. of 15.79 mmol of KNCS to a soln. of 3.94 mmol of UCl4 in 25 ml THF, stirring for 2 hours, addition of 15.79 mmol of the acetamide, stirring for 48 hours; performed under N2;; evapn. to dryness; washing with n-hexane; dissolving in CH2Cl2; centrifugation; concn.; addn. of n-pentane; crystallization within a few hours;washing with n-hexane, n-pentane and drying in vacuum (8 h); elem. anal.;;
DOI:10.1016/0022-5088(84)90390-4

Reference yield: 50.0%

: 93267-72-2
tetrakis(dicyclohexylacetamide)tetraisothiocyanatouranium(IV)

: 93267-70-0
tris(dicyclohexylacetamide)tetraisothiocyanatouranium(IV)

Guidance literature:: In dichloromethane; addition of n-pentane to a solution of the tetrakis-acetamide compound (0.5 g) in 5 ml CH2Cl2; performed under N2;; crystallization within a few hours; washing with n-hexane, n-pentane and drying in vacuum (8 hours); elem. anal.;;
DOI:10.1016/0022-5088(84)90390-4

Reference yield:

: 93267-70-0
tris(dicyclohexylacetamide)tetraisothiocyanatouranium(IV)

: tris(dicyclohexylacetamide)(tetrahydrofuran)tetraisothiocyanatouranium(IV)

Guidance literature:: With tetrahydrofuran; In tetrahydrofuran; ligand coordination in THF;; UV and IR spectroscopy;;
DOI:10.1016/0022-5088(84)90390-4