C₁₇H₁₃BrN₂O₃

Base Information Edit

Chemical Name:C₁₇H₁₃BrN₂O₃
CAS No.:1070503-93-3
Molecular Formula:C₁₇H₁₃BrN₂O₃
Molecular Weight:373.206
Hs Code.:
Mol file:1070503-93-3.mol

C<sub>17</sub>H<sub>13</sub>BrN<sub>2</sub>O<sub>3</sub>

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Chemical Property of C₁₇H₁₃BrN₂O₃ Edit

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Technology Process of C₁₇H₁₃BrN₂O₃

There total 6 articles about C₁₇H₁₃BrN₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 75-52-5
nitromethane

: 1070504-02-7
C₁₆H₁₂BrNO₂

: 1070503-93-3
C₁₇H₁₃BrN₂O₃

Guidance literature:: With ammonium acetate;
DOI:10.1002/chem.201103605

Reference yield:

: 1070503-91-1
C₁₇H₁₄BrNO₃

: 1070503-93-3
C₁₇H₁₃BrN₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / water

1.3: 215 °C

2.1: trichlorophosphate / N,N-dimethyl-formamide

3.1: ammonium acetate

With ammonium acetate; sodium hydroxide; trichlorophosphate; In water; N,N-dimethyl-formamide; 3.1: Henry reaction;
DOI:10.1002/chem.201103605

Reference yield:

: 100-44-7
benzyl chloride

: 1070503-93-3
C₁₇H₁₃BrN₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate

2.1: sodium methylate / methanol

2.2: 160 °C

3.1: sodium hydroxide / water

3.3: 215 °C

4.1: trichlorophosphate / N,N-dimethyl-formamide

5.1: ammonium acetate

With ammonium acetate; sodium methylate; potassium carbonate; sodium hydroxide; trichlorophosphate; In methanol; water; N,N-dimethyl-formamide; 2.1: Hemetsberger indole cyclization / 5.1: Henry reaction;
DOI:10.1002/chem.201103605