Technology Process of C28H24O
There total 4 articles about C28H24O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 30 percent / bromine / CCl4
2: 99 percent Chromat. / AgOTf, 2,6-di-tert-butyl-4-methylpyridine / 24 h / 150 °C
With
2,6-di-tert-butyl-4-methylpyridine; bromine; silver trifluoromethanesulfonate;
In
tetrachloromethane;
DOI:10.1021/jo00146a033
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 85percent H3PO4 / 2 h / 130 °C
2: 30 percent / bromine / CCl4
3: 99 percent Chromat. / AgOTf, 2,6-di-tert-butyl-4-methylpyridine / 24 h / 150 °C
With
2,6-di-tert-butyl-4-methylpyridine; phosphoric acid; bromine; silver trifluoromethanesulfonate;
In
tetrachloromethane;
DOI:10.1021/jo00146a033
- Guidance literature:
-
Multi-step reaction with 4 steps
1: diethyl ether
2: 85percent H3PO4 / 2 h / 130 °C
3: 30 percent / bromine / CCl4
4: 99 percent Chromat. / AgOTf, 2,6-di-tert-butyl-4-methylpyridine / 24 h / 150 °C
With
2,6-di-tert-butyl-4-methylpyridine; phosphoric acid; bromine; silver trifluoromethanesulfonate;
In
tetrachloromethane; diethyl ether;
DOI:10.1021/jo00146a033