chlorotris(3,5-di-tert-butylpyrazolato)(η1-2-(5-phenyltetrazolato))tantalum(V)

Base Information

Chemical Name:chlorotris(3,5-di-tert-butylpyrazolato)(η1-2-(5-phenyltetrazolato))tantalum(V)
CAS No.:387354-58-7
Molecular Formula:C₄₀H₆₂ClN₁₀Ta
Molecular Weight:899.4
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of chlorotris(3,5-di-tert-butylpyrazolato)(η1-2-(5-phenyltetrazolato))tantalum(V)

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Technology Process of chlorotris(3,5-di-tert-butylpyrazolato)(η1-2-(5-phenyltetrazolato))tantalum(V)

There total 1 articles about chlorotris(3,5-di-tert-butylpyrazolato)(η1-2-(5-phenyltetrazolato))tantalum(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: dichlorotris(3,5-di-tert-butylpyrazolato)tantalum(V)

: 29814-09-3
sodium salt of 5-phenyltetrazole

: 387354-58-7
chlorotris(3,5-di-tert-butylpyrazolato)(η1-2-(5-phenyltetrazolato))tantalum(V)

Guidance literature:: In tetrahydrofuran; byproducts: NaCl; Ta-contg. compd. (0.76 mmol), sodium 5-phenyltetrazolate (2.26 mmol) andtetrahydrofuran were charged in a Schlenk flask; stirring at ambient te mp. for 2 h; then the react. mixt. was refluxed for 40 h; under Ar; the volatile compds. were removed under reduced pressure; the solid was extd. with toluene; filtration of toluene ext.; removal of toluene underreduced pressure; recrystn. from hexane at -20°C; elem. anal.;
DOI:10.1021/ic0109389