(CH₃)2C₂NCHN((CH(CH₃)2)2C₆H₃)2CdCH₃

Base Information

• Chemical Name: (CH₃)2C₂NCHN((CH(CH₃)2)2C₆H₃)2CdCH₃
• CAS No.: 1234205-23-2
• Molecular Formula: C₃₀H₄₄CdN₂
• Molecular Weight: 545.103
• Mol file: 1234205-23-2.mol

Synonyms:

Chemical Property of (CH₃)2C₂NCHN((CH(CH₃)2)2C₆H₃)2CdCH₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (CH₃)2C₂NCHN((CH(CH₃)2)2C₆H₃)2CdCH₃

There total 1 articles about (CH₃)2C₂NCHN((CH(CH₃)2)2C₆H₃)2CdCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

dimethylcadmium (506-82-1) + 2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-2-pentene (289618-59-3) → (CH3)2C2NCHN((CH(CH3)2)2C6H3)2CdCH3 (1234205-23-2)

Guidance literature:

In benzene; (under N2, Schlenk); Cd(CH3)2 added to soln. of ligand in benzene, refluxed for 16 h, Cd(CH3)2 added, refluxed for 16 h; volatiles removed in vacuo, extd. into benzene, lyophilized;

DOI:10.1016/j.poly.2010.02.020

Reference yield: 16.0%

(CH3)2C2NCHN((CH(CH3)2)2C6H3)2CdCH3 (1234205-23-2) + tris(pentafluorophenyl)borate (1109-15-5) → HC[C(Me)N(C6H3-2,6-iPr2)]2CdC6F5 (676139-91-6)

Guidance literature:

In benzene; (under N2 or Ar, Schlenk); mixt. of Cd-complex and B(C6F5)3 dissolved inbenzene, stirred at room temp. for 2 h; volatiles removed by lyophilization, residue extd. into pentane, slowly evapd. at -15°C; elem. anal.;

DOI:10.1016/j.poly.2010.02.020

upstream raw materials:

dimethylcadmium

2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-2-pentene

Downstream raw materials:

HC[C(Me)N(C₆H₃-2,6-iPr₂)]2CdC₆F₅