(A,C)-[(η3-allyl)palladium(II)(μ-N,N'-(diethyldithioxbisamidato)-κ-N,N'-Pd-κ-S,S'-Pt)(2-(diphenylphosphino)pyridine)(chloro)platinum(II)]

Base Information

• Chemical Name: (A,C)-[(η3-allyl)palladium(II)(μ-N,N'-(diethyldithioxbisamidato)-κ-N,N'-Pd-κ-S,S'-Pt)(2-(diphenylphosphino)pyridine)(chloro)platinum(II)]
• CAS No.: 281225-80-7
• Molecular Formula: C₂₆H₂₉ClN₃PPdPtS₂
• Molecular Weight: 815.595
• Mol file: 281225-80-7.mol

Synonyms:

Chemical Property of (A,C)-[(η3-allyl)palladium(II)(μ-N,N'-(diethyldithioxbisamidato)-κ-N,N'-Pd-κ-S,S'-Pt)(2-(diphenylphosphino)pyridine)(chloro)platinum(II)]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (A,C)-[(η3-allyl)palladium(II)(μ-N,N'-(diethyldithioxbisamidato)-κ-N,N'-Pd-κ-S,S'-Pt)(2-(diphenylphosphino)pyridine)(chloro)platinum(II)]

There total 2 articles about (A,C)-[(η3-allyl)palladium(II)(μ-N,N'-(diethyldithioxbisamidato)-κ-N,N'-Pd-κ-S,S'-Pt)(2-(diphenylphosphino)pyridine)(chloro)platinum(II)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[(P(C6H5)2(C5H4N))ClPt(H2(C2H5)2N2C2S2)](1+)*Cl(1-)=[(P(C6H5)2(C5H4N))ClPt(H2(C2H5)2N2C2S2)]Cl (281225-74-9) → (A,C)-[(η3-allyl)palladium(II)(μ-N,N'-(diethyldithioxbisamidato)-κ-N,N'-Pd-κ-S,S'-Pt)(2-(diphenylphosphino)pyridine)(chloro)platinum(II)] (281225-80-7)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium bicarbonate / chloroform

2: methanol; chloroform

With sodium bicarbonate; In methanol; chloroform;

DOI:10.1021/om991008o

Reference yield:

bis(η3-allyl-μ-chloropalladium(II)) + [(P(C6H5)2(C5H4N))ClPt(H(C2H5)2N2C2S2)] → (A,C)-[(η3-allyl)palladium(II)(μ-N,N'-(diethyldithioxbisamidato)-κ-N,N'-Pd-κ-S,S'-Pt)(2-(diphenylphosphino)pyridine)(chloro)platinum(II)] (281225-80-7)

Guidance literature:

In methanol; chloroform; soln. was allowed to stand for 2 h; evapd., residue chromd. over Al2O3 (eluent light petroleum), eluate wasconcd., petroleum added, ppt. collected; elem. anal.;

DOI:10.1021/om991008o

upstream raw materials:

[(P(C₆H₅)2(C₅H₄N))ClPt(H₂(C₂H₅)2N₂C₂S₂)]⁽¹⁺⁾*Cl^(1-)=[(P(C₆H₅)2(C₅H₄N))ClPt(H₂(C₂H₅)2N₂C₂S₂)]Cl