diphenylsulfur diimide

Base Information

• Chemical Name: diphenylsulfur diimide
• CAS No.: 3839-89-2
• Molecular Formula: C₁₂H₁₀N₂S
• Molecular Weight: 214.291
• Mol file: 3839-89-2.mol

Synonyms:

Chemical Property of diphenylsulfur diimide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of diphenylsulfur diimide

There total 13 articles about diphenylsulfur diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

aniline (62-53-3) → diphenylsulfur diimide (3839-89-2,66085-13-0,66085-14-1,66085-15-2)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; disulfur dichloride; In chloroform; at -30 ℃; for 2h; Reflux;

DOI:10.1055/s-0032-1318140

Reference yield: 74.0%

C13H8F13NOS (136123-48-3) + aniline (62-53-3) → diphenylsulfur diimide (3839-89-2,66085-13-0,66085-14-1,66085-15-2)

Guidance literature:

In diethyl ether; for 1h;

Reference yield: 69.0%

N-phenylsulfinylamine (222851-56-1) → diphenylsulfur diimide (3839-89-2,66085-13-0,66085-14-1,66085-15-2)

Guidance literature:

With sodium; In toluene; for 2h; Heating;

upstream raw materials:

N-phenylsulfinylamine

aniline

S,S-difluoro-N-phenyl-sulfimide

N-phenyltriphenyliminophosphorane

Downstream raw materials:

2-anilino-3,3-dimethyl-3H-2λ⁴-benzo[c][1,2]thiazin-4-one

N-phenylisobutyramide

2-methyl-N-phenylacrylamide

N,N'-Diphenyl-N-(2-methylpropenoyl)-N'-isobutanoylthiobisamin