1-(6-carboxyhexyl)-2-(3-cyclohexyl-3-hydroxypropyl)-1,2,4-triazolidine-3,5-dione

Base Information

Chemical Name:1-(6-carboxyhexyl)-2-(3-cyclohexyl-3-hydroxypropyl)-1,2,4-triazolidine-3,5-dione
CAS No.:85385-82-6
Molecular Formula:C₁₈H₃₁N₃O₅
Molecular Weight:369.461
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(6-carboxyhexyl)-2-(3-cyclohexyl-3-hydroxypropyl)-1,2,4-triazolidine-3,5-dione

Chemical Property:

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Technology Process of 1-(6-carboxyhexyl)-2-(3-cyclohexyl-3-hydroxypropyl)-1,2,4-triazolidine-3,5-dione

There total 7 articles about 1-(6-carboxyhexyl)-2-(3-cyclohexyl-3-hydroxypropyl)-1,2,4-triazolidine-3,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29823-18-5
ethyl 7-bromoheptanoate

: 85385-82-6
1-(6-carboxyhexyl)-2-(3-cyclohexyl-3-hydroxypropyl)-1,2,4-triazolidine-3,5-dione

Guidance literature:: Multi-step reaction with 7 steps

1: 82 g / sodium hydride, sodium iodide / tetrahydrofuran; hexamethylphosphoric acid triamide; paraffin / 1.) room temperature, 24 h, 2.) reflux, 6 h

2: 16.8 g / hydrogen / 10percent palladium-charcoal / ethanol / 17 h / 5171.5 Torr / Ambient temperature

3: 50 percent / 120 h / Ambient temperature

4: sodium borohydride / ethanol / Ambient temperature

5: 2 N hydrochloric acid / ethanol; H₂O / 24 h / Ambient temperature

6: 1,5-diazabicyclo<5.4.0>undec-5-ene / 12 h / steam bath

7: 2 N sodium hydroxide / H₂O / 3 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; hydrogen; sodium hydride; sodium iodide; 1,5-Diazabicyclo[5.4.0]undec-5-ene; palladium on activated charcoal; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; water; paraffin;
DOI:10.1039/P19810002096

Reference yield:

: 79496-25-6
ethyl 3-benzylidene-2-(6-ethoxycarbonylhexyl)carbazate

: 85385-82-6
1-(6-carboxyhexyl)-2-(3-cyclohexyl-3-hydroxypropyl)-1,2,4-triazolidine-3,5-dione

Guidance literature:: Multi-step reaction with 6 steps

1: 16.8 g / hydrogen / 10percent palladium-charcoal / ethanol / 17 h / 5171.5 Torr / Ambient temperature

2: 50 percent / 120 h / Ambient temperature

3: sodium borohydride / ethanol / Ambient temperature

4: 2 N hydrochloric acid / ethanol; H₂O / 24 h / Ambient temperature

5: 1,5-diazabicyclo<5.4.0>undec-5-ene / 12 h / steam bath

6: 2 N sodium hydroxide / H₂O / 3 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; hydrogen; 1,5-Diazabicyclo[5.4.0]undec-5-ene; palladium on activated charcoal; In ethanol; water;
DOI:10.1039/P19810002096