N⁴--1-(2',3',5'-triacetyl-β-D-arabinosyl)cytosine

Base Information

Chemical Name:N⁴--1-(2',3',5'-triacetyl-β-D-arabinosyl)cytosine
CAS No.:129835-33-2
Molecular Formula:C₂₃H₃₄N₅O₉P
Molecular Weight:555.525
Hs Code.:

N<sup>4</sup>-<bis(2,2-dimethyl-1-aziridinyl)phosphinyl>-1-(2',3',5'-triacetyl-β-D-arabinosyl)cytosine

Synonyms:

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Chemical Property of N⁴--1-(2',3',5'-triacetyl-β-D-arabinosyl)cytosine

Chemical Property:

Purity/Quality:

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Technology Process of N⁴--1-(2',3',5'-triacetyl-β-D-arabinosyl)cytosine

There total 3 articles about N⁴--1-(2',3',5'-triacetyl-β-D-arabinosyl)cytosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2658-24-4
2,2-dimethylaziridine

: C₁₅H₁₈Cl₂N₃O₉P

: 129835-33-2
N⁴--1-(2',3',5'-triacetyl-β-D-arabinosyl)cytosine

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 25 ℃; for 3h; Yield given;
DOI:10.1021/jm00171a039

Reference yield:

: 58227-71-7
1-(2,3,5-tri-O-acetyl-β-D-arabinofuranosyl)cytosine hydrochloride

: 129835-33-2
N⁴--1-(2',3',5'-triacetyl-β-D-arabinosyl)cytosine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Et₃N, 2.) POCl₃, Et₃N / 1.) THF, 25 min, 2.) 0-5 deg C, 45 min

2: Et₃N / tetrahydrofuran / 3 h / 0 - 25 °C

With triethylamine; trichlorophosphate; In tetrahydrofuran;
DOI:10.1021/jm00171a039

Reference yield:

: 147-94-4
arabinosyl cytosine

: 129835-33-2
N⁴--1-(2',3',5'-triacetyl-β-D-arabinosyl)cytosine

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / glacial acetic acid / CHCl₃

2: 1.) Et₃N, 2.) POCl₃, Et₃N / 1.) THF, 25 min, 2.) 0-5 deg C, 45 min

3: Et₃N / tetrahydrofuran / 3 h / 0 - 25 °C

With acetic acid; triethylamine; trichlorophosphate; In tetrahydrofuran; chloroform;
DOI:10.1021/jm00171a039