C₄₄H₇₃N₃O₅Si₂

Base Information

Chemical Name:C₄₄H₇₃N₃O₅Si₂
CAS No.:956223-82-8
Molecular Formula:C₄₄H₇₃N₃O₅Si₂
Molecular Weight:780.252
Hs Code.:

C<sub>44</sub>H<sub>73</sub>N<sub>3</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₄₄H₇₃N₃O₅Si₂

Chemical Property:

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Technology Process of C₄₄H₇₃N₃O₅Si₂

There total 27 articles about C₄₄H₇₃N₃O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 869487-89-8
(S)-3-methyl-6-(trimethylsilyl)hex-5-ynal

: 956223-82-8
C₄₄H₇₃N₃O₅Si₂

Guidance literature:: Multi-step reaction with 12 steps

1: n-BuLi / -78 °C

2: Dess-Martin periodinane; NaHCO₃ / 0 - 20 °C

3: 96 percent / i-Pr₂NEt; LiCl / acetonitrile / 20 °C

4: 92 percent / AD-mix α; MeSO2NH2; NaHCO3 / 2-methyl-propan-2-ol; H2O / 0 °C

5: 95 percent / PPTS / CH₂Cl₂ / 0 - 20 °C

6: K-selectride / tetrahydrofuran / -78 °C

7: NaHMDS / tetrahydrofuran; dimethylformamide / 0 °C

8: TBAF / tetrahydrofuran / 0 - 20 °C

9: Et₃N / CH₂Cl₂ / 0 °C

10: NaN₃ / dimethylformamide / 90 °C

11: CSA / methanol / 0 - 20 °C

12: 2,6-lutidine / 0 °C

With 2,6-dimethylpyridine; AD-mix-α; n-butyllithium; sodium azide; methanesulfonamide; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; potassium tri-sec-butyl-borohydride; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; lithium chloride; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; 4: Sharpless asymmetric dihydroxylation;
DOI:10.1055/s-2007-985585

Reference yield:

: 956223-72-6
C₃₃H₄₄O₄Si

: 956223-82-8
C₄₄H₇₃N₃O₅Si₂

Guidance literature:: Multi-step reaction with 10 steps

1: 96 percent / i-Pr₂NEt; LiCl / acetonitrile / 20 °C

2: 92 percent / AD-mix α; MeSO2NH2; NaHCO3 / 2-methyl-propan-2-ol; H2O / 0 °C

3: 95 percent / PPTS / CH₂Cl₂ / 0 - 20 °C

4: K-selectride / tetrahydrofuran / -78 °C

5: NaHMDS / tetrahydrofuran; dimethylformamide / 0 °C

6: TBAF / tetrahydrofuran / 0 - 20 °C

7: Et₃N / CH₂Cl₂ / 0 °C

8: NaN₃ / dimethylformamide / 90 °C

9: CSA / methanol / 0 - 20 °C

10: 2,6-lutidine / 0 °C

With 2,6-dimethylpyridine; AD-mix-α; sodium azide; methanesulfonamide; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; potassium tri-sec-butyl-borohydride; triethylamine; N-ethyl-N,N-diisopropylamine; lithium chloride; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; 2: Sharpless asymmetric dihydroxylation;
DOI:10.1055/s-2007-985585

Reference yield:

: (R)-2-(dichloromethylene)-4-methyltetrahydro-2H-pyran

: 956223-82-8
C₄₄H₇₃N₃O₅Si₂

Guidance literature:: Multi-step reaction with 17 steps

1: Li / tetrahydrofuran / Heating

2: PPTS / CH₂Cl₂ / 0 - 20 °C

3: n-BuLi / tetrahydrofuran / -78 °C

4: PPTS / methanol / 0 - 20 °C

5: 2-iodoxybenzoic acid / CH₂Cl₂; dimethylsulfoxide / 20 °C

6: n-BuLi / -78 °C

7: Dess-Martin periodinane; NaHCO₃ / 0 - 20 °C

8: 96 percent / i-Pr₂NEt; LiCl / acetonitrile / 20 °C

9: 92 percent / AD-mix α; MeSO2NH2; NaHCO3 / 2-methyl-propan-2-ol; H2O / 0 °C

10: 95 percent / PPTS / CH₂Cl₂ / 0 - 20 °C

11: K-selectride / tetrahydrofuran / -78 °C

12: NaHMDS / tetrahydrofuran; dimethylformamide / 0 °C

13: TBAF / tetrahydrofuran / 0 - 20 °C

14: Et₃N / CH₂Cl₂ / 0 °C

15: NaN₃ / dimethylformamide / 90 °C

16: CSA / methanol / 0 - 20 °C

17: 2,6-lutidine / 0 °C

With 2,6-dimethylpyridine; AD-mix-α; n-butyllithium; sodium azide; methanesulfonamide; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; lithium; sodium hydrogencarbonate; potassium tri-sec-butyl-borohydride; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; lithium chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; 9: Sharpless asymmetric dihydroxylation;
DOI:10.1055/s-2007-985585