C₁₃H₁₈O₄

Base Information

• Chemical Name: C₁₃H₁₈O₄
• CAS No.: 1262789-19-4
• Molecular Formula: C₁₃H₁₈O₄
• Molecular Weight: 238.284
• Mol file: 1262789-19-4.mol

Synonyms:

Chemical Property of C₁₃H₁₈O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₃H₁₈O₄

There total 3 articles about C₁₃H₁₈O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C13H16O4 (1262789-18-3) → C13H18O4 (1262789-19-4)

Guidance literature:

With dimethylsulfide borane complex; In tetrahydrofuran; at 0 - 20 ℃; for 3h; Inert atmosphere;

DOI:10.1021/ja109925g

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) → C13H18O4 (1262789-19-4)

Guidance literature:

Multi-step reaction with 2 steps

1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / Inert atmosphere

2: dimethylsulfide borane complex / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

With dmap; dimethylsulfide borane complex; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja109925g

Reference yield:

4-methylsalicylaldehyde (698-27-1) → C13H18O4 (1262789-19-4)

Guidance literature:

Multi-step reaction with 2 steps

1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / Inert atmosphere

2: dimethylsulfide borane complex / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

With dmap; dimethylsulfide borane complex; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja109925g

upstream raw materials:

C₁₃H₁₆O₄

di-tert-butyl dicarbonate

4-methylsalicylaldehyde

Downstream raw materials:

C₁₆H₂₂O₃

C₁₄H₂₀O