(1,5-Di-O-benzoyl-2,3-O-isopropyliden-β-D-fructopyranosid-4)(exo-benzyl-3,4-O-benzylidene-β-L-arabinopyranosid-2)(2,2,2-trichlorethyl)phosphat

Base Information

Chemical Name:(1,5-Di-O-benzoyl-2,3-O-isopropyliden-β-D-fructopyranosid-4)(exo-benzyl-3,4-O-benzylidene-β-L-arabinopyranosid-2)(2,2,2-trichlorethyl)phosphat
CAS No.:110435-01-3
Molecular Formula:C₄₄H₄₄Cl₃O₁₅P
Molecular Weight:950.157
Hs Code.:

(1,5-Di-O-benzoyl-2,3-O-isopropyliden-β-D-fructopyranosid-4)(exo-benzyl-3,4-O-benzylidene-β-L-arabinopyranosid-2)(2,2,2-trichlorethyl)phosphat

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1,5-Di-O-benzoyl-2,3-O-isopropyliden-β-D-fructopyranosid-4)(exo-benzyl-3,4-O-benzylidene-β-L-arabinopyranosid-2)(2,2,2-trichlorethyl)phosphat

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Technology Process of (1,5-Di-O-benzoyl-2,3-O-isopropyliden-β-D-fructopyranosid-4)(exo-benzyl-3,4-O-benzylidene-β-L-arabinopyranosid-2)(2,2,2-trichlorethyl)phosphat

There total 12 articles about (1,5-Di-O-benzoyl-2,3-O-isopropyliden-β-D-fructopyranosid-4)(exo-benzyl-3,4-O-benzylidene-β-L-arabinopyranosid-2)(2,2,2-trichlorethyl)phosphat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 110434-92-9
1,5-Di-O-benzoyl-2,3-O-isopropyliden-β-D-fructopyranose

: 110434-97-4
(exo-Benzyl-3,4-O-benzyliden-β-L-arabinopyranosid-2)(2,2,2-trichlorethyl)(triethylammonium)phosphat

: 110435-01-3,110507-87-4
(1,5-Di-O-benzoyl-2,3-O-isopropyliden-β-D-fructopyranosid-4)(exo-benzyl-3,4-O-benzylidene-β-L-arabinopyranosid-2)(2,2,2-trichlorethyl)phosphat

Guidance literature:: With MSNT; In pyridine; for 36h; Ambient temperature;

Reference yield:

: 104769-04-2
1-O-Benzoyl-2,3-O-isopropyliden-β-D-fructopyranose

: 110435-01-3,110507-87-4
(1,5-Di-O-benzoyl-2,3-O-isopropyliden-β-D-fructopyranosid-4)(exo-benzyl-3,4-O-benzylidene-β-L-arabinopyranosid-2)(2,2,2-trichlorethyl)phosphat

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 2 h / 0 deg C to RT

3: 1.) p-TsOH 2.) MSNT / 1.) DMF, 4 h, 40 deg C 2.) pyridine, 36 h, RT

With MSNT; toluene-4-sulfonic acid; In pyridine;

Reference yield:

: 7296-55-1
L-arabinose

: 110435-01-3,110507-87-4
(1,5-Di-O-benzoyl-2,3-O-isopropyliden-β-D-fructopyranosid-4)(exo-benzyl-3,4-O-benzylidene-β-L-arabinopyranosid-2)(2,2,2-trichlorethyl)phosphat

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / p-TosOH / 8 h / 60 °C

2: 1.) p-TsOH 2.) MSNT / 1.) DMF, 4 h, 40 deg C 2.) pyridine, 36 h, RT

With MSNT; toluene-4-sulfonic acid;