2--L-leucylamido-2-deoxy-β-D-glucose

Base Information

Chemical Name:2--L-leucylamido-2-deoxy-β-D-glucose
CAS No.:16684-40-5
Molecular Formula:C₂₆H₄₁N₃O₉
Molecular Weight:539.626
Hs Code.:

2-<N-(N-carbobenzyloxy)-L-leucyl>-L-leucylamido-2-deoxy-β-D-glucose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2--L-leucylamido-2-deoxy-β-D-glucose

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Technology Process of 2--L-leucylamido-2-deoxy-β-D-glucose

There total 2 articles about 2--L-leucylamido-2-deoxy-β-D-glucose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7801-71-0
N-benzyloxycarbonyl-L-leucyl-L-leucine

: 16684-40-5
2--L-leucylamido-2-deoxy-β-D-glucose

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) i-BuOCOCl, N-methylmorpholine, 2.) N-methylmorpholine / 1.) THF, -15 deg C, 30 min, 2.) THF, 4 deg C, 15 h

2: 63 percent / NaOMe / tetrahydrofuran; methanol / 0.5 h / -10 - 20 °C

With 4-methyl-morpholine; sodium methylate; isobutyl chloroformate; In tetrahydrofuran; methanol;
DOI:10.1016/0223-5234(91)90001-4

Reference yield:

: 5432-46-2,10034-19-2,10034-20-5,34948-62-4,110253-00-4,1191127-63-5
1,3,4,6-tetra-O-acetyl-D-glucosamine hydrochloride

: 16684-40-5
2--L-leucylamido-2-deoxy-β-D-glucose

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) i-BuOCOCl, N-methylmorpholine, 2.) N-methylmorpholine / 1.) THF, -15 deg C, 30 min, 2.) THF, 4 deg C, 15 h

2: 63 percent / NaOMe / tetrahydrofuran; methanol / 0.5 h / -10 - 20 °C

With 4-methyl-morpholine; sodium methylate; isobutyl chloroformate; In tetrahydrofuran; methanol;
DOI:10.1016/0223-5234(91)90001-4