allyl O-(3-acetyl-4-azido-4,6-dideoxy-3-C-methyl-2-O-methyl-α-L-mannopyranosyl)-(1->3)-O-(4-O-benzoyl-2-O-methyl-α-D-rhamnopyranosyl)-(1->3)-4-O-benzoyl-2-O-methyl-α-L-fucopyranoside

Base Information

Chemical Name:allyl O-(3-acetyl-4-azido-4,6-dideoxy-3-C-methyl-2-O-methyl-α-L-mannopyranosyl)-(1->3)-O-(4-O-benzoyl-2-O-methyl-α-D-rhamnopyranosyl)-(1->3)-4-O-benzoyl-2-O-methyl-α-L-fucopyranoside
CAS No.:137226-40-5
Molecular Formula:C₄₁H₅₃N₃O₁₅
Molecular Weight:827.883
Hs Code.:

allyl O-(3-acetyl-4-azido-4,6-dideoxy-3-C-methyl-2-O-methyl-α-L-mannopyranosyl)-(1->3)-O-(4-O-benzoyl-2-O-methyl-α-D-rhamnopyranosyl)-(1->3)-4-O-benzoyl-2-O-methyl-α-L-fucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl O-(3-acetyl-4-azido-4,6-dideoxy-3-C-methyl-2-O-methyl-α-L-mannopyranosyl)-(1->3)-O-(4-O-benzoyl-2-O-methyl-α-D-rhamnopyranosyl)-(1->3)-4-O-benzoyl-2-O-methyl-α-L-fucopyranoside

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Technology Process of allyl O-(3-acetyl-4-azido-4,6-dideoxy-3-C-methyl-2-O-methyl-α-L-mannopyranosyl)-(1->3)-O-(4-O-benzoyl-2-O-methyl-α-D-rhamnopyranosyl)-(1->3)-4-O-benzoyl-2-O-methyl-α-L-fucopyranoside

There total 7 articles about allyl O-(3-acetyl-4-azido-4,6-dideoxy-3-C-methyl-2-O-methyl-α-L-mannopyranosyl)-(1->3)-O-(4-O-benzoyl-2-O-methyl-α-D-rhamnopyranosyl)-(1->3)-4-O-benzoyl-2-O-methyl-α-L-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 137226-35-8
3-O-acetyl-4-azido-4,6-dideoxy-3-C-methyl-2-O-methyl-α-L-mannopyranosyl trichloroacetimidate

: 137226-22-3
allyl O-(4-O-benzoyl-2-O-methyl-α-D-rhamnopyranosyl)-(1->3)-4-O-benzoyl-2-O-methyl-α-L-fucopyranoside

: 137226-40-5
allyl O-(3-acetyl-4-azido-4,6-dideoxy-3-C-methyl-2-O-methyl-α-L-mannopyranosyl)-(1->3)-O-(4-O-benzoyl-2-O-methyl-α-D-rhamnopyranosyl)-(1->3)-4-O-benzoyl-2-O-methyl-α-L-fucopyranoside

Guidance literature:: With 4 A molecular sieve; boron trifluoride diethyl etherate;
DOI:10.1016/0008-6215(92)84173-P

Reference yield:

: 137226-34-7
3-O-acetyl-4-azido-4,6-dideoxy-3-C-methyl-2-O-methyl-α,β-L-mannopyranose

: 137226-40-5
allyl O-(3-acetyl-4-azido-4,6-dideoxy-3-C-methyl-2-O-methyl-α-L-mannopyranosyl)-(1->3)-O-(4-O-benzoyl-2-O-methyl-α-D-rhamnopyranosyl)-(1->3)-4-O-benzoyl-2-O-methyl-α-L-fucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / 1,5-diazabicyclo<5.4.0>undec-5-ene / CH₂Cl₂ / 0.33 h / Ambient temperature

2: 89 percent / 4 Angstroem molecular sieves, BF₃*Et₂O

With 4 A molecular sieve; boron trifluoride diethyl etherate; 1,5-Diazabicyclo[5.4.0]undec-5-ene; In dichloromethane;
DOI:10.1016/0008-6215(92)84173-P

Reference yield:

: 137226-33-6
1,3-di-O-acetyl-4-azido-4,6-dideoxy-3-C-methyl-2-O-methyl-α-L-mannopyranose

: 137226-40-5
allyl O-(3-acetyl-4-azido-4,6-dideoxy-3-C-methyl-2-O-methyl-α-L-mannopyranosyl)-(1->3)-O-(4-O-benzoyl-2-O-methyl-α-D-rhamnopyranosyl)-(1->3)-4-O-benzoyl-2-O-methyl-α-L-fucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / hydrazine acetate / dimethylformamide / 24 h / Ambient temperature

2: 97 percent / 1,5-diazabicyclo<5.4.0>undec-5-ene / CH₂Cl₂ / 0.33 h / Ambient temperature

3: 89 percent / 4 Angstroem molecular sieves, BF₃*Et₂O

With 4 A molecular sieve; boron trifluoride diethyl etherate; hydrazinium monoacetate; 1,5-Diazabicyclo[5.4.0]undec-5-ene; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(92)84173-P