Technology Process of C38(13)C4H68N8O11
There total 12 articles about C38(13)C4H68N8O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
2: palladium on carbon; hydrogen / ethanol
3: acetonitrile / 72 h / Reflux
4: trifluoroacetic acid / dichloromethane / 3 h
5: acetic anhydride / 3 h / 120 °C
6: acetonitrile / 60 h / Reflux
7: trifluoroacetic acid / dichloromethane / 3 h
With
palladium on carbon; hydrogen; acetic anhydride; trifluoroacetic acid;
In
ethanol; dichloromethane; acetonitrile;
DOI:10.1021/ja1097034
- Guidance literature:
-
Multi-step reaction with 6 steps
1: palladium on carbon; hydrogen / ethanol
2: acetonitrile / 72 h / Reflux
3: trifluoroacetic acid / dichloromethane / 3 h
4: acetic anhydride / 3 h / 120 °C
5: acetonitrile / 60 h / Reflux
6: trifluoroacetic acid / dichloromethane / 3 h
With
palladium on carbon; hydrogen; acetic anhydride; trifluoroacetic acid;
In
ethanol; dichloromethane; acetonitrile;
DOI:10.1021/ja1097034
- Guidance literature:
-
Multi-step reaction with 9 steps
1: hydrogenchloride; water / Reflux
2: acetic anhydride
4: palladium on carbon; hydrogen / ethanol
5: acetonitrile / 72 h / Reflux
6: trifluoroacetic acid / dichloromethane / 3 h
7: acetic anhydride / 3 h / 120 °C
8: acetonitrile / 60 h / Reflux
9: trifluoroacetic acid / dichloromethane / 3 h
With
hydrogenchloride; palladium on carbon; water; hydrogen; acetic anhydride; trifluoroacetic acid;
In
ethanol; dichloromethane; acetonitrile;
DOI:10.1021/ja1097034