Technology Process of C68H93N5O6
There total 7 articles about C68H93N5O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium permanganate; sodium hydroxide / water / 90 - 95 °C
2.1: thionyl chloride / toluene / 3 h / Heating
2.2: Cooling with ice; Reflux
With
potassium permanganate; thionyl chloride; sodium hydroxide;
In
water; toluene;
DOI:10.1080/15421400903065754
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: aluminum (III) chloride
2.1: hydrazine
3.1: aluminum (III) chloride; acetyl chloride
4.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C
4.2: 1 h / 0 °C
5.1: thionyl chloride / toluene / 3 h / Heating
5.2: Cooling with ice; Reflux
With
hydrogenchloride; aluminum (III) chloride; thionyl chloride; acetyl chloride; hydrazine; sodium nitrite;
In
water; toluene;
3.2: Schmidt reaction;
DOI:10.1080/15421400903065754
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C
1.2: 1 h / 0 °C
2.1: thionyl chloride / toluene / 3 h / Heating
2.2: Cooling with ice; Reflux
With
hydrogenchloride; thionyl chloride; sodium nitrite;
In
water; toluene;
DOI:10.1080/15421400903065754
