3-amino-5-cyano-1,1-dimethylindane

Base Information

Chemical Name:3-amino-5-cyano-1,1-dimethylindane
CAS No.:142559-86-2
Molecular Formula:C₁₂H₁₄N₂
Molecular Weight:186.257
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-amino-5-cyano-1,1-dimethylindane

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Technology Process of 3-amino-5-cyano-1,1-dimethylindane

There total 5 articles about 3-amino-5-cyano-1,1-dimethylindane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 142559-85-1
3-Azido-5-cyano-1,1-dimethylindane

: 142559-86-2,1213591-14-0
3-amino-5-cyano-1,1-dimethylindane

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; under 760 Torr;
DOI:10.1021/jm00011a016

Reference yield:

: 64278-20-2
1,1-Dimethyl-indan-5-carbonitrile

: 142559-86-2,1213591-14-0
3-amino-5-cyano-1,1-dimethylindane

Guidance literature:: Multi-step reaction with 3 steps

1: NBS, AIBN / CCl₄ / 0.5 h / Heating; Irradiation

2: sodium azide / dimethylformamide / 4 h / Ambient temperature

3: H₂ / 10percent Pd/C / ethanol / 760 Torr

With N-Bromosuccinimide; sodium azide; 2,2'-azobis(isobutyronitrile); hydrogen; palladium on activated charcoal; In tetrachloromethane; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00011a016

Reference yield:

: 124369-43-3
1,1-Dimethyl-1H-indene-5-carbonitrile

: 142559-86-2,1213591-14-0
3-amino-5-cyano-1,1-dimethylindane

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 10percent Pd/C / ethanol / 760 Torr

2: NBS, AIBN / CCl₄ / 0.5 h / Heating; Irradiation

3: sodium azide / dimethylformamide / 4 h / Ambient temperature

4: H₂ / 10percent Pd/C / ethanol / 760 Torr

With N-Bromosuccinimide; sodium azide; 2,2'-azobis(isobutyronitrile); hydrogen; palladium on activated charcoal; In tetrachloromethane; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00011a016