[Rh(DIPAMP)(β-methyl succinate)]

Base Information

• Chemical Name: [Rh(DIPAMP)(β-methyl succinate)]
• CAS No.: 1217367-43-5
• Molecular Formula: C₃₃H₃₃O₆P₂Rh
• Molecular Weight: 690.474

Synonyms:

Chemical Property of [Rh(DIPAMP)(β-methyl succinate)]

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of [Rh(DIPAMP)(β-methyl succinate)]

There total 2 articles about [Rh(DIPAMP)(β-methyl succinate)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methylenesuccinic acid (97-65-4,25119-64-6) + [Rh(DIPAMP)(MeOH)2]BF4 → [Rh(DIPAMP)(β-methyl succinate)] (1217367-43-5)

Guidance literature:

With triethyl amine; In methanol; diethyl ether; under Ar, Schlenk techniques; 0.01 mmol (Rh(DIPAMP)(MeOH)2)BF4 and 0.05 mmol itaconic acid in MeOH by slow diffusion of Et2O or by addition of 0.05 mmol Et3N; (31)P NMR spect.;

DOI:10.1016/j.jorganchem.2010.12.020

Reference yield:

2-methylenesuccinic acid (97-65-4,25119-64-6) + [Rh(DIPAMP)(BF4)]2 → [Rh(DIPAMP)(β-methyl succinate)] (1217367-43-5)

Guidance literature:

In methanol; under Ar, Schlenk techniques; orange soln. fades within a few minutes, room temp.; (31)P NMR spect.;

DOI:10.1016/j.jorganchem.2010.12.020

upstream raw materials:

2-methylenesuccinic acid

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