Technology Process of C22H32N2O8
There total 7 articles about C22H32N2O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydride; tetra-(n-butyl)ammonium iodide / mineral oil; tetrahydrofuran / 0 - 20 °C
2: sodium azide; acetic acid / N,N-dimethyl-formamide / Reflux
3: ammonium formate; palladium 10% on activated carbon / methanol / 48 h / Reflux
4: sodium hydrogencarbonate / methanol / 6 h / 0 °C
With
sodium azide; palladium 10% on activated carbon; ammonium formate; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; acetic acid;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.tetasy.2012.12.005
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium azide; acetic acid / N,N-dimethyl-formamide / 48 h / 95 °C
2: ammonium formate; palladium 10% on activated carbon / methanol / 48 h / Reflux
3: sodium hydrogencarbonate / methanol / 6 h / 0 °C
With
sodium azide; palladium 10% on activated carbon; ammonium formate; sodium hydrogencarbonate; acetic acid;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2012.12.005
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ammonium formate; palladium 10% on activated carbon / methanol / 48 h / Reflux
2: sodium hydrogencarbonate / methanol / 6 h / 0 °C
With
palladium 10% on activated carbon; ammonium formate; sodium hydrogencarbonate;
In
methanol;
DOI:10.1016/j.tetasy.2012.12.005
