Technology Process of C40H64O6SSi
There total 21 articles about C40H64O6SSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C16H22O2S;
With
n-butyllithium;
In
tetrahydrofuran;
at -78 ℃;
for 0.333333h;
C24H42O4Si;
at -78 - 20 ℃;
for 1h;
DOI:10.1271/bbb.130243
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 0.33 h / 0 - 20 °C
2.1: N,N-dimethyl-formamide / 0 - 20 °C
3.1: n-butyllithium / tetrahydrofuran / 0.33 h / -78 °C
3.2: 1 h / -78 - 20 °C
With
n-butyllithium; carbon tetrabromide; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1271/bbb.130243
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N,N-dimethyl-formamide / 0 - 20 °C
2.1: n-butyllithium / tetrahydrofuran / 0.33 h / -78 °C
2.2: 1 h / -78 - 20 °C
With
n-butyllithium;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1271/bbb.130243