3-Fluorobenzaldehyde N-phenylthiosemicarbazone

Base Information

Chemical Name:3-Fluorobenzaldehyde N-phenylthiosemicarbazone
CAS No.:16113-69-2
Molecular Formula:C₁₄H₁₂FN₃S
Molecular Weight:273.334
Hs Code.:
European Community (EC) Number:656-004-3

Synonyms:AKOS003451708;3-FLUOROBENZALDEHYDE N-PHENYLTHIOSEMICARBAZONE

Suppliers and Price of 3-Fluorobenzaldehyde N-phenylthiosemicarbazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-Fluorobenzaldehyde N-phenylthiosemicarbazone

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:273.07359673
Heavy Atom Count:19
Complexity:316

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)NC(=S)NN=CC2=CC(=CC=C2)F
Isomeric SMILES:C1=CC=C(C=C1)NC(=S)N/N=C/C2=CC(=CC=C2)F

Technology Process of 3-Fluorobenzaldehyde N-phenylthiosemicarbazone

There total 2 articles about 3-Fluorobenzaldehyde N-phenylthiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1240952-24-2
2,4-bis(3-fluorophenyl)-3-azabicyclo[3.3.1]nonan-9-one

: 5351-69-9
4-Phenyl-3-thiosemicarbazide

: 16113-69-2
C₁₄H₁₂FN₃S

: C₂₇H₂₆F₂N₄S

Guidance literature:: In ethanol; chloroform; at 90 - 100 ℃; for 96h; Acidic conditions;
DOI:10.3109/14756366.2010.525508

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 456-48-4
3-Fluorobenzaldehyde

: 16113-69-2
C₁₄H₁₂FN₃S

: C₂₇H₂₆F₂N₄S

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium acetate / ethanol / 20 °C

2: ethanol; chloroform / 96 h / 90 - 100 °C / Acidic conditions

With ammonium acetate; In ethanol; chloroform;
DOI:10.3109/14756366.2010.525508