Technology Process of C37H68N2O2
There total 6 articles about C37H68N2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 70 percent / p-toluenesulfonic acid / toluene / Heating
2: lithium hydroxide monohydrate / methanol / 16 h
3: lithium hydroxide monohydrate / tetrahydrofuran
4: 7.35 g / oxalyl chloride / tetrahydrofuran; dimethylformamide
5: diisopropylethylamine / tetrahydrofuran
6: 74 percent / LiAlH4 / tetrahydrofuran / Heating
With
lithium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetasy.2004.09.004
- Guidance literature:
-
Multi-step reaction with 5 steps
1: lithium hydroxide monohydrate / methanol / 16 h
2: lithium hydroxide monohydrate / tetrahydrofuran
3: 7.35 g / oxalyl chloride / tetrahydrofuran; dimethylformamide
4: diisopropylethylamine / tetrahydrofuran
5: 74 percent / LiAlH4 / tetrahydrofuran / Heating
With
lithium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2004.09.004