[bis(triphenylphosphine)iminium](1+)*[Fe4(NO)4(μ3-S)2(μ3-NCMe3)2](1-)

Base Information

Chemical Name:[bis(triphenylphosphine)iminium](1+)*[Fe4(NO)4(μ3-S)2(μ3-NCMe3)2](1-)
CAS No.:80399-52-6
Molecular Formula:C₈H₁₈Fe₄N₆O₄S₂*C₃₆H₃₀NP₂
Molecular Weight:1088.38
Hs Code.:

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Suppliers and Price of [bis(triphenylphosphine)iminium](1+)*[Fe4(NO)4(μ3-S)2(μ3-NCMe3)2](1-)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [bis(triphenylphosphine)iminium](1+)*[Fe4(NO)4(μ3-S)2(μ3-NCMe3)2](1-)

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Technology Process of [bis(triphenylphosphine)iminium](1+)*[Fe4(NO)4(μ3-S)2(μ3-NCMe3)2](1-)

There total 1 articles about [bis(triphenylphosphine)iminium](1+)*[Fe4(NO)4(μ3-S)2(μ3-NCMe3)2](1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53276-79-2
Fe4(NO)4(μ3-S)2(μ3-NC(CH3)3)2

: bis(triphenylphosphine)iminium chloride

: 80399-52-6
[bis(triphenylphosphine)iminium](1+)*[Fe4(NO)4(μ3-S)2(μ3-NCMe3)2](1-)

Guidance literature:: With sodium amalgame; In tetrahydrofuran; Fe complex in THF soln. added dropwise to sodium amalgame/THF soln.; stirred 5 min; filtered 3x; (Ph3P)2NCl/acetone soln. added to filtrate; stirred 30 min; all procedures under N2 or Ar; solvent vac. removed; extd. with THF; crystd. by slow diffusion with THF and heptane; all steps under N2 or Ar;
DOI:10.1021/ja00367a017