C₂₂H₃₀O₈

Base Information

Chemical Name:C₂₂H₃₀O₈
CAS No.:1586000-27-2
Molecular Formula:C₂₂H₃₀O₈
Molecular Weight:422.475
Hs Code.:

C<sub>22</sub>H<sub>30</sub>O<sub>8</sub>

Synonyms:

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Chemical Property of C₂₂H₃₀O₈

Chemical Property:

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Technology Process of C₂₂H₃₀O₈

There total 11 articles about C₂₂H₃₀O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1586000-25-0
(S,E)-5-{(4S,5S)-5-[(S)-1-hydroxybut-3-ynyl]-2,2-dimethyl-1,3-dioxolan-4-yl}pent-4-en-2-ol

: 1586000-27-2
C₂₂H₃₀O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: silver nitrate; N-Bromosuccinimide / acetone / 1 h

2.1: bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 0.5 h / 20 °C

3.1: bis(dibenzylideneacetone)-palladium⁽⁰⁾; lithium chloride; triphenyl-arsane / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

3.2: 2 h / 60 °C / Inert atmosphere

4.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 24 h

With bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; lithium hydroxide monohydrate; triphenyl-arsane; water; silver nitrate; lithium chloride; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; N,N-dimethyl-formamide; acetone; 3.1: |Stille Cross Coupling / 3.2: |Stille Cross Coupling;
DOI:10.1016/j.tet.2014.03.001

Reference yield:

: 23568-31-2
2,3:4,5-di-O-isopropylidene-L-arabinose

: 1586000-27-2
C₂₂H₃₀O₈

Guidance literature:: Multi-step reaction with 11 steps

1.1: potassium tert-butylate / tetrahydrofuran / 1.33 h / 0 - 20 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: water; acetic acid / 20 °C

3.1: di(n-butyl)tin oxide; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: potassium carbonate; methanol / 3 h / 20 °C / Inert atmosphere

5.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 24 h / Inert atmosphere; Reflux

6.1: n-butyllithium / tetrahydrofuran; hexane / -78 - 0 °C / Inert atmosphere

6.2: 0.33 h / -78 °C / Inert atmosphere

6.3: 1 h / -78 °C / Inert atmosphere

7.1: potassium carbonate; methanol / 12 h / 20 °C

8.1: silver nitrate; N-Bromosuccinimide / acetone / 1 h

9.1: bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 0.5 h / 20 °C

10.1: bis(dibenzylideneacetone)-palladium⁽⁰⁾; lithium chloride; triphenyl-arsane / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

10.2: 2 h / 60 °C / Inert atmosphere

11.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 24 h

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; methanol; bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; n-butyllithium; lithium hydroxide monohydrate; triphenyl-arsane; potassium tert-butylate; water; di(n-butyl)tin oxide; potassium carbonate; silver nitrate; acetic acid; triethylamine; lithium chloride; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; acetone; 1.1: |Wittig Olefination / 1.2: |Wittig Olefination / 10.1: |Stille Cross Coupling / 10.2: |Stille Cross Coupling;
DOI:10.1016/j.tet.2014.03.001

Reference yield:

: 1574334-59-0
(S)-1-((4S,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)ethane-1,2-diol

: 1586000-27-2
C₂₂H₃₀O₈

Guidance literature:: Multi-step reaction with 9 steps

1.1: di(n-butyl)tin oxide; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: potassium carbonate; methanol / 3 h / 20 °C / Inert atmosphere

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 24 h / Inert atmosphere; Reflux

4.1: n-butyllithium / tetrahydrofuran; hexane / -78 - 0 °C / Inert atmosphere

4.2: 0.33 h / -78 °C / Inert atmosphere

4.3: 1 h / -78 °C / Inert atmosphere

5.1: potassium carbonate; methanol / 12 h / 20 °C

6.1: silver nitrate; N-Bromosuccinimide / acetone / 1 h

7.1: bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 0.5 h / 20 °C

8.1: bis(dibenzylideneacetone)-palladium⁽⁰⁾; lithium chloride; triphenyl-arsane / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

8.2: 2 h / 60 °C / Inert atmosphere

9.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 24 h

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; methanol; bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; n-butyllithium; lithium hydroxide monohydrate; triphenyl-arsane; water; di(n-butyl)tin oxide; potassium carbonate; silver nitrate; triethylamine; lithium chloride; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; acetone; 8.1: |Stille Cross Coupling / 8.2: |Stille Cross Coupling;
DOI:10.1016/j.tet.2014.03.001